Fatigue mechanisms at 450°C of a highly twined (>70%) and HIP-densified IN718 superalloy additively manufactured by laser beam powder bed fusion
Source abstract
Abstract
Fatigue resistance at elevated temperatures is crucial for certifying aerospace structures additively manufactured by the laser beam powder bed fusion (PBF-LB) method with IN718 superalloy. This study employed a multi-step, supersolvus heat treatment process with hot isostatic pressing (HIP), called RHSA, to minimize pores and brittle phases. Stress intensity factor (△K) calculations using data from X-ray computed tomography and shape factors referencing finite element analysis (FEA) studies confirmed the suppression of △K below the threshold of conventional IN718 (∼5 MPa√m), shifting fatigue behavior to grain-structure-dominated. Despite a very high twin boundary (TB) fraction (>70%), fatigue tests at 450°C and R = 0.1 demonstrated low scatter. Slip trace analysis and high-resolution electron backscatter diffraction (EBSD) revealed that TB-induced strain concentration became prominent only at high △K, causing cracking at 45⁰ to the loading direction. The randomly oriented TBs with higher angles (60⁰) compared to high-angle grain boundaries (HAGBs) (30–40⁰) likely enhanced slip resistance and provided a net strengthening effect, which can explain the lower-than-average TB% along fracture paths. These insights suggest that a high TB fraction is not detrimental if fatigue stress is not excessive, alleviating concerns about annealing twins during defect minimization in AM IN718, allowing novel processes to improve fatigue resistance in PBF-LB IN718.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · Additive Manufacturing and 3D Printing Technologies · High Entropy Alloys Studies
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (58)
Show source-provided references
1. B.G. Muralidharan, V. Shankar. Weldability of Inconel 718 - A Review. 1996.
2. Precipitation around welds in the nickel-base superalloy, Inconel 71810.1016/0001-6160(85)90231-7 ↗
3. ASM International, ASM Specialty Handbook: Nickel, Cobalt, and Their Alloys, ASM International. 2000.
4. Inferior fatigue resistance of additively-manufactured Ni-based superalloy 718 and its dominating factor10.1016/j.ijfatigue.2023.107801 ↗
5. Estimation of order strengthening in inconel 718 type alloys containing all γ″ precipitate variants10.1016/0956-716X(93)90165-O ↗
6. J.W. Brooks, P.J. Bridges, Metallurgical Stability of Inconel Alloy 718, 1988. https://doi.org/10.7449/1988/Superalloys_1988_33_42.10.7449/1988/Superalloys_1988_33_42 ↗
7. Morphology of y’ and y“ precipitates and thermal stability of inconel 718 type alloys10.1007/BF02649604 ↗
8. The effect of δ phase on the mechanical properties of an Inconel 718 superalloy10.1007/s11665-012-0433-7 ↗
9. Studies of standard heat treatment effects on microstructure and mechanical properties of laser net shape manufactured INCONEL 71810.1007/s11661-009-9949-3 ↗
10. N. KAWAGOISHI, Q. CHEN, H. NISITANI, Kawagoishi, Chen, Nisitani, N. KAWAGOISHI, Q. CHEN, H. NISITANI, Fatigue strength of Inconel 718 at elevated temperatures, Fatigue & Fracture of Engineering Materials & Structures. 23 (2000) 209–216. https://doi.org/https://doi.org/10.1046/j.1460-2695.2000.00263.x.10.1046/j.1460-2695.2000.00263.x ↗
11. Four point bending fatigue property of Ni-base superalloy Udimet 720Li10.2472/jsms.46.1389 ↗
12. Special Metals Corporation, INCONEL alloy. 718. 2007.
13. Effect of grain size and notch on high cycle fatigue strength of a nickel-base superalloy at elevated temperature10.1299/kikaia.50.1443 ↗
14. The superalloys fundamentals and applications
15. A review of mechanical properties of additively manufactured Inconel 718
16. Long fatigue crack growth in Inconel 718 produced by selective laser melting10.1016/j.ijfatigue.2016.03.012 ↗
17. Effect of anisotropy and texture on the low cycle fatigue behavior of Inconel 718 processed via electron beam melting10.1016/j.ijfatigue.2017.08.021 ↗
18. Additive manufacturing of fatigue resistant materials: Challenges and opportunities10.1016/j.ijfatigue.2017.01.001 ↗
19. P.F.K. Jr., Fatigue Behavior of Direct Metal Laser Sintered (DMLS) Inconel 718, Tufts University. 2015.
20. Multiaxial fatigue of Inconel 718 produced by Selective Laser Melting at room and high temperature10.1016/j.ijfatigue.2022.107108 ↗
21. The influence of Laves phases on the high-cycle fatigue behavior of laser additive manufactured Inconel 71810.1016/j.msea.2017.03.098 ↗
22. Anisotropy in cyclic behavior and fatigue crack growth of IN718 processed by laser powder bed fusion
23. Unnotched fatigue of Inconel 718 produced by laser beam-powder bed fusion at 25 and 600 °C10.1016/j.actamat.2021.117565 ↗
24. Fatigue behavior and microstructural evolution of additively manufactured Inconel 718 under cyclic loading at elevated temperature10.1016/j.ijfatigue.2020.105598 ↗
25. Microstructure, fatigue, and impact toughness properties of additively manufactured nickel alloy 718
26. Notched fatigue testing of Inconel 718 prepared by selective laser melting10.1111/ffe.12880 ↗
27. Knowledge of process-structure-property relationships to engineer better heat treatments for laser powder bed fusion additive manufactured Inconel 718
28. Effects of post-processing route on fatigue performance of laser powder bed fusion Inconel 718
29. Hot isostatic pressing of IN718 components manufactured by selective laser melting
30. Creep property of Inconel 718 superalloy produced by selective laser melting compared to forging10.1016/j.msea.2020.139947 ↗
31. Low cycle fatigue behavior of direct metal laser sintered Inconel alloy10.1016/j.ijfatigue.2016.08.019 ↗
32. A review on the fatigue cracking of twin boundaries : Crystallographic orientation and stacking fault energy10.1016/j.pmatsci.2022.101011 ↗
33. Atomistic observation of a crack tip approaching coherent twin boundaries
34. D. Texier, J.-C. Stinville, M.-A. Charpagne, Z. Chen, V. Valle, P. Villechaise, T.M. Pollock, J. Cormier, Role of Non-metallic Inclusions and Twins on the Variability in Fatigue Life in Alloy 718 Nickel Base Superalloy, in: S. Tin, M. Hardy, J. Clews, J. Cormier, Q. Feng, J. Marcin, C. O’Brien, A. Suzuki (Eds.), Superalloys 2020, Springer International Publishing, Cham, 2020: pp. 629–639.10.1007/978-3-030-51834-9_61 ↗
35. Role of precipitates-decorated Σ3 twin boundaries on hydrogen-induced crack initiation and propagation in Ni-based superalloy 71810.1016/j.corsci.2023.111189 ↗
36. Evolution of the annealing twin density during δ-supersolvus grain growth in the nickel-based superalloy Inconel 718
37. ASTM International, Standard Specification for Additive Manufacturing Nickel Alloy (UNS N07718) with Powder Bed Fusion. 2021.
38. S. Specification, A. Manufacturing, N. Alloy, Standard Specification for Additive Manufacturing Nickel Alloy (UN... http://www.astm.org/FULL_TEXT/F3055/HTML/F3055.htm#s00001, (n.d.) 1–17.
39. SAE International, Heat Treatment Nickel Alloy and Cobalt Alloy Parts AMS2774G. 2000.
40. ASTM International, ASTM E466-15: Standard Practice for Conducting Force Controlled Constant Amplitude Axial Fatigue Tests of Metallic Materials, 2016. https://doi.org/10.1520/E0466-15.2.
41. MTex, Slip Systems, (2024). https://mtex-toolbox.github.io/SlipSystems.html.
42. Stored energy density research on the fatigue crack initiation at twin boundary and life prediction of Inconel718 superalloy10.1016/j.ijfatigue.2023.107590 ↗
43. Impact of high temperature stress relieving on final properties of Inconel 718 processed by laser powder bed fusion10.1016/j.msea.2021.141111 ↗
44. Effect of heat treatment on the modification of microstructure of selective laser melted (SLM) IN718 and its consequences on mechanical behavior10.1557/jmr.2020.129 ↗
45. Enhanced strength of additively manufactured Inconel 718 by means of a simplified heat treatment strategy10.1016/j.jmatprotec.2023.118197 ↗
46. Influence of high initial porosity introduced by laser powder bed fusion on the fatigue strength of Inconel 718 after post-processing with hot isostatic pressing
47. On the constitutive relationship between solidification cells and the fatigue behaviour of IN718 fabricated by laser powder bed fusion
48. Current theoretical approaches to collective behavior of dislocations10.1016/j.physrep.2006.10.003 ↗
49. The Portevin-Le Chatelier effect: A review of experimental findings10.1088/1468-6996/12/6/063001 ↗
50. Schijve · 2009
51. Stress-intensity factor solutions for embedded elliptical cracks in round bars subjected to tensile load10.1016/j.tafmec.2021.103189 ↗
52. B.H. Lawless, A.W. Dix, Effect of Processing/Microstructure on the Threshold Fatigue Crack Growth Behaviour of Alloy 718 Forging, in: Superalloys 2001, 2001.10.7449/2001/Superalloys_2001_553_564 ↗
53. Fatigue crack propagation in nickel-base superalloys – Effects of microstructure, load ratio, and temperature10.1179/mst.1987.3.9.750 ↗
54. Effects of grain size and precipitate size on the fatigue crack growth behavior of alloy 718 at 427 °C10.1007/BF02646657 ↗
55. A dislocation model for fatigue crack initiation10.1115/1.3157599 ↗
56. MTEX, Grain Reference Orientation Deviation (GROD), (2023). https://mtex-toolbox.github.io/EBSDGROD.html.
57. Oxford Instruments Plc., GROD Angle Maps. 2021.
58. The role of slip transfer at grain boundaries in the propagation of microstructurally short fatigue cracks in Ni-based superalloys10.1016/j.scriptamat.2018.11.008 ↗