Mechanical properties of hot‐pressed transparent platelet alumina
Source abstract
Abstract
Abstract The mechanical properties of transparent alumina densified by hot‐pressing platelet‐morphology powder were characterized and compared to samples using equiaxed (E) powder. The platelet alumina was prepared in two different starting orientations prior to hot‐pressing. In the first, the platelets were poured into the die in a non‐pre‐aligned (NPA) state. In the second, the platelets were pre‐aligned (PA) via a separate processing step. The characteristic strength of the NPA, PA, and E samples is 179, 206, and 207 MPA, respectively. The Weibull modulus of the NPA samples is m = 24, which is among the highest Weibull modulus reported for alumina. The Weibull modulus of the NPA samples is higher than the PA and E samples ( m = 7 and m = 4, respectively) and is explained by a tighter grain size distribution. The Vickers hardness of the NPA, PA, and E samples were measured both parallel and perpendicular to the hot‐pressing direction, with values on the order of 17 GPa, and minimal differences among different samples types. However, the pre‐aligned samples exhibited hardness values nearly identical to sapphire in the corresponding crystallographic directions. This is due to the pre‐alignment procedure resulting in significant crystallographic orientation in the final sintered parts.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Advanced ceramic materials synthesis · Ferroelectric and Piezoelectric Materials · Advanced materials and composites
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
School of Materials Engineering Purdue University West Lafayette Indiana USA
Funding
Army Research Office
References (34)
Show source-provided references
1. Krell A · 2005 · 1
2. 10.1016/j.optmat.2008.12.00910.1016/j.optmat.2008.12.009 ↗
3. 10.1111/j.1151-2916.2003.tb03270.x10.1111/j.1151-2916.2003.tb03270.x ↗
4. Parish MV · 2017 · 1
5. 10.1117/1.OE.56.7.07710310.1117/1.OE.56.7.077103 ↗
6. 10.1111/j.1151-2916.2003.tb03325.x10.1111/j.1151-2916.2003.tb03325.x ↗
7. WachtmanJ CannonW MatthewsonM.Mechanical properties of ceramics. 2nd ed. Hoboken NJ: John Wiley & Sons Inc.;2009.65–69 191–193 210–216 p.2009.
8. 10.1016/j.ceramint.2012.03.07410.1016/j.ceramint.2012.03.074 ↗
9. 10.1016/j.jeurceramsoc.2018.02.00610.1016/j.jeurceramsoc.2018.02.006 ↗
10. 10.1016/0955-2219(95)90350-R10.1016/0955-2219(95)90350-R ↗
11. 10.3103/S106287380910017710.3103/S1062873809100177 ↗
12. 10.1111/jace.1693210.1111/jace.16932 ↗
13. 10.1111/jace.1704410.1111/jace.17044 ↗
14. 10.1016/j.ceramint.2021.10.03110.1016/j.ceramint.2021.10.031 ↗
15. 10.3390/app1113614510.3390/app11136145 ↗
16. 10.1179/09679789968026410.1179/096797899680264 ↗
17. 10.1111/j.1151-2916.1999.tb02123.x10.1111/j.1151-2916.1999.tb02123.x ↗
18. RhodesWH SellersDJ HeuerAH VasilofT.Development and evaluation of transparent aluminum oxide. Avco Corporation Lowell MA;1967.10.21236/AD0661487 ↗
19. SchlupA.Processing aluminum oxide for the control of microstructral texture and optical properties. West Lafayette IN: Purdue University;2020.
20. Standard test method for flexural strength of advanced ceramics at ambient temperature
21. ASTM International. ASTM standard C693 1993 (2013) standard test method for density of glass by buoyancy. West Conshohocken PA: ASTM International;2013.
22. ASTM. Standard practice for reporting uniaxial strength data and estimating Weibull distribution parameters for advanced ceramics. West Conshohocken PA: ASTM; 2000.
23. ASTM International · 2015
24. 10.1038/nmeth.201910.1038/nmeth.2019 ↗
25. 10.1016/j.msea.2010.03.03510.1016/j.msea.2010.03.035 ↗
26. HeuerAH RhodesWH SellersDJ VasilosT.Microstructure studies of polycrystalline refractory oxides. Avco Corporation Lowell MA;1967.
27. 10.1016/j.matlet.2018.03.12310.1016/j.matlet.2018.03.123 ↗
28. 10.1016/j.jeurceramsoc.2020.03.07310.1016/j.jeurceramsoc.2020.03.073 ↗
29. 10.1111/j.1151-2916.1997.tb03074.x10.1111/j.1151-2916.1997.tb03074.x ↗
30. 10.1016/0955-2219(95)91430-V10.1016/0955-2219(95)91430-V ↗
31. 10.1016/j.ceramint.2017.11.09810.1016/j.ceramint.2017.11.098 ↗
32. 10.1111/j.1151-2916.1991.tb06884.x10.1111/j.1151-2916.1991.tb06884.x ↗
33. 10.2109/jcersj.100.135710.2109/jcersj.100.1357 ↗
34. 10.1111/j.1151-2916.1995.tb08871.x10.1111/j.1151-2916.1995.tb08871.x ↗