journal article·2017-05Open access

Densification and characterization of rapid carbothermal synthesized boron carbide

Muhammet Fatih Toksoy, William Rafaniello, Kelvin Yu Xie, Luoning Ma, Kevin Jude Hemker, Richard Alan Haber

Abstract

Abstract Submicrometer boron carbide powders were synthesized using rapid carbothermal reduction (RCR) method. Synthesized boron carbide powders had smaller particle size, lower free carbon, and high density of twins compared to commercial samples. Powders were sintered using spark plasma sintering at different temperatures and dwell times to compare sintering behavior. Synthesized boron carbide powders reached >99% TD at lower temperature and shorter dwell times compared to commercial powders. Improved microhardness observed in the densified RCR samples was likely caused by the combination of higher purity, better stoichiometry control, finer grain size, and a higher density of twin boundaries.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Boron and Carbon Nanomaterials Research · Advanced materials and composites

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Mechanical Engineering Izmir Institute of Technology Urla Izmir Turkey

Materials Sci. & Eng Rutgers University New Brunswick NJ USA

Mechanical Engineering Johns Hopkins University Baltimore MD USA

Funding

Army Research Laboratory · Defense Advanced Research Projects Agency · National Science Foundation

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