Supramolecular Isomerism in Cadmium Hydroxide Phases. Temperature-Dependent Synthesis and Structure of Photoluminescent Coordination Polymers of α- and β-Cd2(OH)2(2,4-pyda)
Source abstract
Abstract
Two isomeric inorganic−organic hybrid materials formulated as [Cd 2 (OH) 2 (2,4-pyda)] (2,4-pyda = 2,4-pyridinedicarboxylate) have been hydrothermally synthesized via transformation of one-dimensional coordination chains formulated as [Cd(H 2 O) 2 (2,4-pyda)] into three-dimensional coordination polymers at different temperatures and characterized by crystallography.
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Research context
OpenAlex topics: Metal-Organic Frameworks: Synthesis and Applications · Crystal structures of chemical compounds · Crystallography and molecular interactions
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
School of Chemistry and Chemical Engineering & State Key Laboratory of Optoelectronic Materials and Technologies, Sun Yat-Sen University, Guangzhou 510275, P. R. China, Department of Synthetical Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia
References (26)
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15. X-ray single-crystal diffraction data collections were collected on a Rigaku/MSC Mercury CCD diffractometer for1and3and on a Bruker Smart Apex CCD diffractometer for2with graphite-monochromated Mo Kα radiation (λ= 0.71073 Å). Crystal data for1: orthorhombic, space groupPbca,a= 12.137(7) Å,b= 7.742(5) Å,c= 18.618(9) Å,V= 1749.5(18) Å3,Z= 8, ρalcd= 2.381 g cm-3, (Mo Kα) = 25.06 cm-1.R1= 0.0391,wR2= 0.0939 (for all data). Crystal data for2: monoclinic, space groupP21/c,a= 10.4291(9) Å,b= 6.0983(5) Å,c= 15.2762(13) Å, β = 106.992(2)°,V= 929.15(14) Å3,Z= 4, ρalcd= 3.030 g cm-3, (Mo Kα) = 45.88 cm-1.R1= 0.0220,wR2= 0.0508 (for all data). Crystal data for3: monoclinic, space groupP21/c,a= 10.523(6) Å,b= 11.065(8) Å,c= 8.061(4) Å, β = 94.643(12)°,V= 935.5(10) Å3,Z= 4, ρalcd= 3.010 g cm-3, (Mo Kα) = 45.57 cm-1.R1= 0.0211,wR2= 0.0725 (for all data).
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