Photoluminescent Zn(II) Metal−Organic Frameworks Built from Tetrazole Ligand: 2D Four-Connected Regular Honeycomb (4363)-net
Source abstract
Abstract
Two metal−organic frameworks, [Zn 2 (ATA) 3 (ATA) 2/2 ] ( 1 ) and [Zn(OH)(ATA) 2 ] ( 2 ), have been synthesized by the hydrothermal reactions of Zn(II) salts with HATA. 1 displays a unique four-connected 2D bilayer “hcb” 4 3 .6 3 topological network, and shows a strong blue fluorescence at room temperature.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Metal-Organic Frameworks: Synthesis and Applications · Magnetism in coordination complexes · Covalent Organic Framework Applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Faculty of Materials Science and Chemical Engineering, China University of Geoscience, Hubei, Wuhan 370007, P. R. China, and College of Chemistry and Chemical Engineering, Shengzhen University, Guangdong, Shengzhen 518060, P. R. China
References (64)
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45. Preparation of1: The mixture of Zn(NO3)2·6H2O (0.285 g, 1.0 mmol), HATA (0.108 g, 1.0 mmol), and H2O (18.0 ml) was sealed in a 25 ml stainless-steel reactor with Teflon liner; it was heated to 160 °C, kept at constant temperature for 120 h, and then slowly cooled to room temperature. Colorless block crystals of [Zn2(ATA)3(ATA)2/2] (1) were abtained (yield: 65% based on the initial HATA input). Anal. Calcd for C4H7Zn2N20(%): C, 10.28; H, 1.71; N, 59.95. Found: C, 10.25; H, 1.65; N, 59.93. IR data (cm-1, KBr): 3341s, 3195s, 1655s, 1606s, 1571s, 1471s, 1448m, 1421m, 1375m, 1331w, 1166w, 1094m, 1007w, 905w, 786w, 754w, 494s.
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61. Preparation of2: The mixture of ZnSO4·6H2O (0.269 g, 1.0 mmol), HATA (0.108 g, 1.0 mmol), NaOH (0.040 g, 1.0 mmol), and H2O (18.0 ml) was sealed in a 25 mL stainless-steel reactor with Teflon liner; it was heated to 160 °C, kept at constant temperature for 120 h, and then slowly cooled to room temperature. Colorless rod-shaped crystals of [Zn(OH)(ATA)] (2) were abtained (yield: 85% based on the initial ZnSO4·6H2O input). Anal. Calcd for CH3ZnN5O (%): C, 7.21; H, 1.80; N, 42.05. Found: C, 7.25; H, 1.86; N, 42.02. IR data (cm-1, KBr): 3397s, 3338s, 3245s, 3204s, 1663s, 1587s, 1571s, 1506w, 1471s, 1448m, 1396w, 1302w, 1160w, 1112m, 1094s, 1015m, 905s, 833w, 765w, 748w, 489s.
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