Size-Controllable Growth of Single Crystal In(OH)₃ and In₂O₃ Nanocubes

Single crystal In(OH) 3 nanocubes were synthesized by a designed novel hydrothermal treatment, and the size can be simply moderated by varying the hydrothermal temperature. By calcining the In(OH) 3 nanocubes in air at 400 °C, single crystal In 2 O 3 nanocubes were also prepared with the size slightly shrinking. Room temperature photoluminescence showed a broad photoluminescence emission spectrum in the blue-green region with its maximum intensity centered at 450 nm, which was mainly attributed to the effect of the oxygen deficiencies.