journal article·2020-02Open access

On the suitability of slow strain rate tensile testing for assessing hydrogen embrittlement susceptibility

Emilio Martínez-Pañeda, Zachary D. Harris, Sandra Fuentes-Alonso, John R. Scully, James T. Burns

Corrosion Science· Volume 163

Abstract

The onset of sub-critical crack growth during slow strain rate tensile testing (SSRT) is assessed through a combined experimental and modeling approach. A systematic comparison of the extent of intergranular fracture and expected hydrogen ingress suggests that hydrogen diffusion alone is insufficient to explain the intergranular fracture depths observed after SSRT experiments in a Ni–Cu superalloy. Simulations of these experiments using a new phase field formulation indicate that crack initiation occurs as low as 40% of the time to failure. The implications of such sub-critical crack growth on the validity and interpretation of SSRT metrics are then explored.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Hydrogen embrittlement and corrosion behaviors in metals · Nuclear Materials and Properties · High Temperature Alloys and Creep

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (100+)

Show source-provided references
1. Hydrogen-assisted cracking
2. Critical issues in hydrogen assisted cracking of structural alloys
3. Hydrogen embrittlement understood10.1007/s11663-015-0325-y ↗
4. Discussion of some recent literature on hydrogen-embrittlement mechanisms: addressing common misunderstandings10.1515/corrrev-2019-0017 ↗
5. Modeling hydrogen induced damage mechanisms in metals
6. Strain gradient plasticity-based modeling of hydrogen environment assisted cracking10.1016/j.actamat.2016.07.022 ↗
7. Elucidating the contribution of mobile hydrogen-deformation interactions to hydrogen-induced intergranular cracking in polycrystalline nickel10.1016/j.actamat.2018.07.043 ↗
8. Probabilistic fracture mechanics simulation of stress corrosion cracking using accelerated laboratory testing and multi-scale modeling10.5006/1920 ↗
9. Raja · 2011
10. NACE Standard MR01795-98, Sulfide Stress Cracking Resistant Metallic Materials for Oilfield Equipment, NACE International, Houston, TX.
11. NACE TM0198, Slow Strain Rate Test Method for Screening Corrosion-Resistant Alloys (CRAs) for Stress Corrosion Cracking in Sour Oilfield Service, NACE International, Houston, TX.
12. ASTM G30, Standard Practice for Making and Using U-Bend Stress-Corrosion Test Specimens, ASTM International, West Conshohocken, PA.
13. ASTM G39, Standard Practice for Preparation and Use of Bent-Beam Stress-Corrosion Test Specimens, ASTM International, West Conshohocken, PA.
14. ASTMG129-00, Standard Practice for Slow Strain Rate Testing to Evaluate the Susceptibility of Metallic Materials to Environmentally Assisted Cracking, ASTM International, West Conshohocken, PA.
15. ASTM E1681-03, Standard Test Method for Determining Threshold Stress Intensity Factor for Environment-Assisted Cracking of Metallic Materials, ASTM International, West Conshohocken, PA.
16. ASTM F1624-12, Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique, ASTM International, West Conshohocken, PA.
17. ISO 7539-7, Corrosion of Metals and Alloys – Stress Corrosion Testing – Part 7: Method for Slow Strain Rate Testing, International Organization for Standardization.
18. A review of the constant strain-rate stress corrosion cracking test
19. Ugiansky · 1979
20. Kane · 1993
21. The slow strain rate stress corrosion cracking test – a 50 year retrospective10.5006/2137 ↗
22. Slow strain rate testing for materials evaluation in high-pressure H2S environments10.5006/1.3584966 ↗
23. Verification of the development of low hydrogen embrittling zinc–nickel electroplate by slow strain rate testing10.1016/0026-0576(95)95845-8 ↗
24. Slow strain-rate technique: application to caustic stress corrosion cracking studies
25. Hydrogen cracking initiation of a high-strength steel weldment
26. Problems associated with slow strain rate quality assurance testing of nickel-base corrosion resistant alloy tubulars in hydrogen sulfide environments
27. Limitations of the slow strain rate test for stress corrosion cracking testing10.5006/1.3315931 ↗
28. Improved SSR test for lot acceptance criterion
29. Statistical treatment of slow strain rate data for assessment of hydrogen embrittlement in high strength 4340 steel10.1016/0010-938X(92)90165-Y ↗
30. Ranking materials for extreme sour gas service using the slow strain rate method
31. Effects of testing variables on stress corrosion cracking susceptibility of Al 2024-T35110.1016/j.corsci.2011.09.021 ↗
32. The application of the slow strain rate test method for the development of linepipe steels resistant to sulphide stress cracking10.1016/0010-938X(87)90095-3 ↗
33. Influence of surface condition on primary water stress corrosion cracking initiation of alloy 60010.5006/1.3290356 ↗
34. Anderson · 2005
35. Estimation of environment-induced crack growth rate as a function of stress intensity factors generated during slow strain rate testing of aluminum alloys
36. Improved understanding of environment-induced cracking (EIC) of sensitized 5XXX series aluminium alloys10.1016/j.msea.2016.11.088 ↗
37. Deformation rate and sensitization effects on environmentally assisted cracking of Al–Mg naval alloys10.5006/1949 ↗
38. Initiation and growth of stress corrosion cracks in type 316L stainless steel during slow strain rate testing10.5006/1.3293468 ↗
39. Incremental damage formulation for stress corrosion cracking and its application to crack growth interpretation based on CERT data10.5006/1.3585053 ↗
40. Acoustic emission monitoring of slow strain rate tensile tests of 304L stainless steel in supercritical water environment10.1016/j.corsci.2010.09.006 ↗
41. Estimation of crack initiation stress and local fracture toughness of Ni-alloys 945X (UNS N09946) and 718 (UNS N07718) under hydrogen environment via fracture surface topography analysis10.1016/j.engfracmech.2017.12.010 ↗
42. The effect of heat-to-heat variations in metallurgy and hydrogen-metal interactions on the hydrogen embrittlement of Monel K-50010.1016/j.msea.2017.07.019 ↗
43. The effect of microstructural variation on the hydrogen environment-assisted cracking of Monel K-50010.1007/s11661-016-3486-7 ↗
44. Precipitation in the Ni–Cu-base alloy Monel K-50010.1016/0025-5416(86)90236-3 ↗
45. A century of Monel metal: 1906–200610.1007/s11837-006-0077-x ↗
46. Precipitation hardening in nickel–copper base alloy Monel K 50010.1007/BF02659495 ↗
47. Davis · 2000
48. Coarsening of TiC in austenitic stainless steel – experiments and simulations in comparison10.1016/S0921-5093(00)00827-3 ↗
49. 2000
50. Monel K-500 hydrogen embrittlement
51. Hydrogen diffusion and trapping in a precipitation-hardened nickel–copper–aluminum alloy Monel K-500 (UNS N05500)10.1016/j.actamat.2013.02.007 ↗
52. Measurement and modeling of hydrogen environment-assisted cracking in Monel K-50010.1007/s11661-014-2324-z ↗
53. A phase field formulation for hydrogen assisted cracking10.1016/j.cma.2018.07.021 ↗
54. On fracture in finite strain gradient plasticity10.1016/j.ijplas.2015.09.009 ↗
55. Non-local plasticity effects on notch fracture mechanics10.1016/j.tafmec.2017.09.007 ↗
56. The role of plastic strain gradients in the crack growth resistance of metals10.1016/j.jmps.2019.02.011 ↗
57. Harris · 2013
58. Measurement and modeling of hydrogen environment-assisted cracking in a Ni–Cu–Al–Ti superalloy10.1007/s11661-015-3315-4 ↗
59. Efird · 1985
60. Failures of nickel/copper bolts in subsea application10.2118/16632-PA ↗
61. Hydrogen embrittlement of cathodically protected subsea bolting alloys
62. A quantum-mechanically informed continuum model of hydrogen embrittlement10.1016/j.jmps.2004.02.010 ↗
63. Prevention of hydrogen embrittlement in steels10.2355/isijinternational.ISIJINT-2015-430 ↗
64. Example of the effect of hydrogen trapping on hydrogen embrittlement10.1007/BF02648348 ↗
65. Hydrogen embrittlement of grain boundaries in nickel: an atomistic study10.1038/s41524-017-0031-1 ↗
66. Hydrogen embrittlement in nickel, visited by first principles modeling, cohesive zone simulation and nanomechanical testing10.1016/j.ijhydene.2015.06.069 ↗
67. Bourdin · 2008
68. Phase-field modelling of fracture10.1016/bs.aams.2019.08.001 ↗
69. A phase-field/gradient damage model for brittle fracture in elastic–plastic solids10.1016/j.ijplas.2014.09.005 ↗
70. A phase-field model for solute-assisted brittle fracture in elastic–plastic solids10.1016/j.ijplas.2017.11.004 ↗
71. Phase field modeling of ductile fracture at finite strains: a variational gradient-extended plasticity-damage theory10.1016/j.ijplas.2016.04.011 ↗
72. A uniform hydrogen degradation law for high strength steels10.1016/j.engfracmech.2016.02.001 ↗
73. Crack growth resistance in metallic alloys: the role of isotropic versus kinematic hardening10.1115/1.4040696 ↗
74. Shewmon · 2016
75. Thermodynamics of stress-induced interstitial redistribution in body-centered cubic metals10.1007/s11661-003-0183-0 ↗
76. Strain gradient plasticity modeling of hydrogen diffusion to the crack tip10.1016/j.ijhydene.2016.05.014 ↗
77. On the kinetics of intergranular embrittlement of nickel by hydrogen transport from the external surface10.1016/0036-9748(87)90438-8 ↗
78. Grain size and grain-boundary effects on diffusion and trapping of hydrogen in pure nickel10.1016/j.actamat.2012.09.004 ↗
79. Accelerated diffusion of hydrogen along grain boundaries in nickel10.1016/1359-6454(95)00446-7 ↗
80. Grain boundary transport of hydrogen in nickel10.1016/0036-9748(82)90273-3 ↗
81. Segregation and diffusion of hydrogen in grain boundaries of palladium10.1016/0036-9748(87)90423-6 ↗
82. Grain boundary diffusion of hydrogen in nickel10.1007/BF02656803 ↗
83. SIMS study of hydrogen at the surface and grain boundaries of nickel bicrystals10.1016/0001-6160(87)90150-7 ↗
84. Intercrystalline hydrogen transport in nanocrystalline nickel10.1016/0956-716X(91)90114-G ↗
85. Hydrogen diffusion and permeation in micro- and nanocrystalline nickel10.1016/0956-7151(93)90051-S ↗
86. The influence of intercrystalline defects on hydrogen activity and transport in nickel10.1016/0956-7151(95)00019-R ↗
87. Effects of grain-boundary networks on the macroscopic diffusivity of hydrogen in polycrystalline materials10.1016/j.commatsci.2014.10.048 ↗
88. Is hydrogen diffusion along grain boundaries fast or slow? Atomistic origin and mechanistic modeling10.1103/PhysRevLett.122.215501 ↗
89. Energetics and kinetics of hydrogen at the grain boundary of the Ni alloys: a first-principles study10.1016/j.jallcom.2019.05.030 ↗
90. First-principles investigation of hydrogen trapping and diffusion at grain boundaries in nickel10.1016/j.actamat.2015.07.031 ↗
91. Molecular dynamics studies of irradiation effects on hydrogen isotope diffusion through nickel crystals and grain boundaries10.1039/C7CP06086F ↗
92. Experimental studies of grain boundary diffusion of hydrogen in metals10.1016/0956-7151(91)90333-V ↗
93. Hydrogen diffusion and intergranular cracking in nickel10.1016/S0360-3199(97)00001-3 ↗
94. Hydrogen gas embrittlement
95. An analysis of ductile rupture in notched bars10.1016/0022-5096(84)90031-0 ↗
96. 2004
97. Modelling of the hydrogen distribution at a crack tip10.1016/0921-5093(95)09897-6 ↗
98. Hydrogen in metals: a coupled theory for species diffusion and large elastic–plastic deformations10.1016/j.ijplas.2012.11.005 ↗
99. Coupled hydrogen diffusion simulation using a heat transfer analogy10.1016/j.ijmecsci.2016.07.020 ↗
100. Gradient plasticity crack tip characterization by means of the extended finite element method10.1007/s00466-017-1375-6 ↗