journal article·2017-10

Multiscale investigation of crack path and microstructural changes during liquid metal embrittlement of 304L austenitic steel in liquid sodium

B. Barkia, T. Auger, J.L Courouau, J. Bourgon

Corrosion Science· Volume 127
Publisher page

Abstract

Abstract Fracture micro-mechanisms and crack path of embrittled austenitic steel 304L by liquid sodium strained at 4.2 × 10−7 m s−1 and 573 K are investigated underneath the fracture surface by transmission electron microscopy down to the nanoscale. Automated crystal orientation and phase mapping analyses show that abundant martensitic transformation (γ austenite → α’ martensite) as well as mechanical twinning occur during the deformation of austenite and play a major role in the fracture process. A correlation between the fracture surface features and the underlying microstructural interfaces is evidenced, strengthening the conclusion that liquid metal embrittlement by sodium of austenitic steels is basically an interfacial cracking phenomenon.
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Research context

OpenAlex topics: Hydrogen embrittlement and corrosion behaviors in metals · High Temperature Alloys and Creep · Microstructure and Mechanical Properties of Steels

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References (33)

Show source-provided references
1. Effect of oxygen on liquid sodium embrittlement of T91 martensitic steel10.1016/j.corsci.2013.07.018 ↗
2. Multiscale investigation of quasi-brittle fracture characteristics in a9Cr–1Mo ferritic–martensitic steel embrittled by liquid lead–bismuth under low cycle fatigue10.1016/j.corsci.2015.10.003 ↗
3. Effect of heat treatment on liquid sodium embrittlement of T91 martensitic steel10.1016/j.jmatprotec.2011.07.006 ↗
4. The liquid metal embrittlement of iron and ferritic steels in sodium10.1016/0010-938X(95)92861-E ↗
5. Liquid metal embrittlement of type 316L stainless austenitic steel by gallium as measured by elasto-plastic fracture mechanics10.5006/1.3287729 ↗
6. Action du zinc liquide sur les aciers au nickel
7. Liquid metal embrittlement of an austenitic 316L type and a ferritic–martensitic T91 type steel by mercury10.1016/j.jnucmat.2008.02.032 ↗
8. Liquid metal embrittlement of an austenitic stainless steel in liquid sodium10.1016/j.corsci.2014.02.031 ↗
9. On the formation and nature of quasi-cleavage fracture surfaces in hydrogen embrittled steels10.1016/j.actamat.2010.11.024 ↗
10. Automatic crystal orientation and phase mapping in TEM by precession diffraction
11. Corrosion by liquid sodium of materials for sodium fast reactors: the CORRONa testing device
12. Single crystal and sintered alumina corrosion in liquid sodium
13. Deformation induced martensitic phase transformation in stainless steel of 304L
14. Cleavage step formation in brittle fracture
15. Die Entstehung zungenartiger Stufen auf Spaltflächen
16. Direct observations of martensite nuclei in stainless steel10.1016/0001-6160(79)90074-9 ↗
17. Deformation-induced martensitic characteristics in 304 and 316 stainless steels during room-temperature rolling10.1007/BF02663916 ↗
18. Kurdjumov · Zeitschrift für Physik · 1930 · 64 · 32510.1007/BF01397346 ↗
19. Quantitative measurement of deformation-induced martensite in 304 stainless steel by X-ray diffraction10.1016/j.scriptamat.2004.03.011 ↗
20. Epsilon and α’ martensite formation and reversion in austenitic stainless steels
21. Cleavage-like fracture of austenite in duplex stainless steel10.1016/0956-716X(93)90300-H ↗
22. Nature of gallium focused ion beam induced phase transformation in 316L austenitic stainless steel10.1016/j.actamat.2016.08.008 ↗
23. Stacking fault energies of seven commercial austenitic stainless steels10.1007/BF02641927 ↗
24. A general mechanism of martensitic nucleation: part I. General concepts and the FCC→HCP transformation
25. Correlations between the calculated stacking fault energy and the plasticity mechanisms in Fe–Mn–C alloys
26. Effects of deformation induced phase transformation and twinning on the mechanical properties of austenitic Fe–Mn–Al alloys10.2355/isijinternational.29.868 ↗
27. Martensitic transformations induced by plastic deformation in the Fe-Ni-Cr-C system
28. Influence of flowing sodium on creep deformation and rupture behaviour of 316L(N) austenitic stainless steel10.1016/j.jnucmat.2012.04.030 ↗
29. A microstructural based understanding of hydrogen-enhanced fatigue of stainless steels10.1016/j.ijfatigue.2012.08.009 ↗
30. Deformation structures developing on fine scales10.1080/14786430310001605560 ↗
31. Twin boundary-accelerated ferritization of austenitic stainless steels in liquid lead–bismuth eutectic10.1016/j.scriptamat.2016.02.029 ↗
32. Study of grain boundary character along intergranular stress corrosion crack paths in austenitic alloys10.1016/S1359-6454(01)00064-7 ↗
33. The control of brittleness and development of desirable mechanical properties in polycrystalline systems by grain boundary engineering10.1016/S1359-6454(99)00275-X ↗