journal article·2022-09

One-step preparation and ablation behavior of ZrC-SiC-Si coating for nose-shaped ZrC/C composites with gradient pore structure by vapor silicon infiltration

Ningning Yan, Jiaping Zhang, Tianyu Liu, Wei Xie, Qiangang Fu, Jia Sun, Qingliang Shen

Corrosion Science· Volume 206
Publisher page

Abstract

To improve the ablation resistance of the nose-shaped ZrC/C composites with gradient pore structure (ZrC/C GS ), a ZrC-SiC-Si coating was prepared by one-step vapor silicon infiltration. The bonding strength between the ZrC-SiC-Si coating and the ZrC/C GS composite was 21.2 MPa. The hardness and elastic modulus of the ZrC-SiC-Si coating were 1650.5 ± 30.5 HV and 176.7 ± 3.2 GPa. As the temperature increased from 200 to 1500 ℃, the CTE of the ZrC-SiC-Si coated ZrC/C GS composites increased from 4.9 × 10 −6 K −1 to 6.18 × 10 −6 K −1 . After ablation for 40 s using oxyacetylene torch with a heat flux 2.4 MW/m 2 , the linear ablation rate of the ZrC-SiC-Si coated ZrC/C GS composites decreased by 54.8% compared with that of the ZrC/C GS composites, and it could be maintained at 97.4% of the original heat resistance capacity. The finite element simulation results showed that the residual thermal stresses at the coating/matrix interface were in the range of 10.7–20.2 MPa. After ablation for 40 × 3 s, the ZrC-SiC-Si coating failed.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · MXene and MAX Phase Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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