Corrosion resistance of AISI 316L coated with an air-cured hydrogen silsesquioxane based spin-on-glass enamel in chloride environment
Source abstract
Abstract
Abstract The efficiency of thin hydrogen silsesquioxane (HSQ) −based corrosion barrier coatings on 316L substrates after oxidative thermal curing at 400–550 °C in air was investigated. Infrared spectroscopy and electrochemical impedance spectroscopy showed that an increasing curing temperature leads to progressing coating densification, accompanied by decreasing barrier properties. Cyclic polarization measurements indicated that defects due to substrate oxidation are detrimental for the substrate passivity. Insufficiently polymerized coatings showed poor chemical stability in neutral salt spray testing and the chemical coating stability increased with curing temperature. Oxidative curing was found inadequate as polymerization treatment of HSQ-based corrosion barrier coatings on 316L substrate.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Corrosion Behavior and Inhibition · Hydrogen embrittlement and corrosion behaviors in metals · Metal and Thin Film Mechanics
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (64)
Show source-provided references
1. The initiation of crevice corrosion in stainless steel10.1016/S0010-938X(97)00050-4 ↗
2. Crevice corrosion of stainless steels in sodium chloride solution10.1016/0010-938X(78)90030-6 ↗
3. Crevice corrosion of stainless-steel fastening components in an indoor marine-water basin
4. Failure investigation of heat exchanger plates due to pitting corrosion10.1016/j.engfailanal.2009.10.023 ↗
5. Enhancement of corrosion protection of AISI 304 stainless steel by nanostructured sol–gel TiO2 films10.1016/j.corsci.2013.07.045 ↗
6. Improvement in corrosion protection properties of TiO2 coatings by chromium doping10.1016/j.corsci.2012.10.040 ↗
7. Polyindole top coat on TiO2 sol–gel films for corrosion protection of steel10.1016/j.corsci.2012.08.067 ↗
8. Corrosion studies of stainless steel protected by a TiO2 thin film deposited on a sulfonate-functionalized self-assembled monolayer10.1016/j.corsci.2009.08.052 ↗
9. Pitting of AISI 304L stainless steel coated with nano structured sol–gel alumina coatings in chloride containing acidic environments10.1016/j.corsci.2009.08.037 ↗
10. Corrosion resistance of stainless steel coated with sol–gel silica10.1016/S0022-3093(00)00155-1 ↗
11. Protection of 316L stainless steel against corrosion by SiO2 coatings10.1007/BF00633520 ↗
12. Protective glass coatings on metallic substrates10.1016/0022-3093(90)90155-F ↗
13. Two layered silica protective film made by a spray-and-dip coating method on 304 stainless steel10.1007/s10971-010-2234-5 ↗
14. Electrochemical behaviour enhancement of stainless steels by a SiO2 PACVD coating10.1016/j.corsci.2008.01.015 ↗
15. Fabrication of continuous mesoporous organic–inorganic nanocomposite films for corrosion protection of stainless steel in PEM fuel cells10.1016/j.corsci.2011.01.020 ↗
16. Synthesis and properties of microporous sol?gel silica membranes10.1016/S0022-3093(00)00163-0 ↗
17. Vitreous enamel
18. Modified stainless steel surfaces targeted to reduce fouling − evaluation of fouling by milk components10.1016/j.jfoodeng.2006.09.008 ↗
19. Modified stainless steel surfaces targeted to reduce fouling–surface characterization10.1016/j.jfoodeng.2003.09.013 ↗
20. Chemical vapor deposition of silicon dioxide films
21. Sintering
22. Thermal curing of hydrogen silsesquioxane10.1149/1.1393196 ↗
23. Cure of hydrogen silsesquioxane for intermetal dielectric applications10.1557/PROC-476-37 ↗
24. Properties of a-SiOx:H thin films deposited form hydrogen silsesquioxane resins10.1149/1.1838726 ↗
25. A study on the surface roughness of a thin HSQ coating on a fine milled surface
26. Verification of thickness and surface roughness of a thin film transparent coating
27. Pranov · 2013
28. Surface roughness reduction using spray-coated hydrogen silsesquioxane reflow10.1016/j.apsusc.2013.05.004 ↗
29. Hydrogen silsesquioxane mold coatings for improved replication of nanopatterns by injection molding10.1088/0960-1317/25/3/035018 ↗
30. Pranov · 2014
31. Hydrogen Silsesquioxane based silica glass coatings for the corrosion protection of austenitic stainless steel10.1016/j.surfcoat.2016.10.020 ↗
32. Low-dielectric constant insulators for future integrated circuits and packages10.1146/annurev-chembioeng-061010-114137 ↗
33. Interfacial interaction of oxidatively cured hydrogen silsesquioxane spin-on-glass enamel with stainless steel substrate10.1149/2.0681706jes ↗
34. New electrochemical cell for pitting corrosion testing
35. EN ISO 9227:2012 · 2012
36. The oligomeric silsesquioxanes, (HSiO3/2)n10.1021/ja00722a009 ↗
37. Materials issues with thin film hydrogen silsesquioxane low K dielectrics10.1149/1.1838907 ↗
38. Comparison of properties of dielectric films deposited by various methods10.1116/1.569413 ↗
39. Adsorption of water on silica10.1038/2231150a0 ↗
40. Analysis of the corrosion protective ability of PACVD silica-based coatings deposited on steel10.1016/j.surfcoat.2005.11.130 ↗
41. High temperature oxidation resistance and corrosion properties of dip coated silica coating by sol gel method on stainless steel10.1007/s10971-012-2786-7 ↗
42. Effects of sol-gel coatings on the localized corrosion behavior of 304 stainless steel10.1149/1.1837589 ↗
43. 2016
44. Assessment of intergranular corrosion of heat treated austenitic stainless steel (AISI 316L grade) by electron microscopy and electrochemical tests10.1134/S0033173208050172 ↗
45. Selective oxidation of a ferritic stainless steel and its influence on resistance to crevice corrosion initiation10.1016/0010-938X(81)90038-X ↗
46. Role of heat tint on pitting corrosion of 304 austenitic stainless steel in chloride environmen
47. Technical note: concerning the conversion of the constant phase element parameter Y0 into a capacitance10.5006/1.3280607 ↗
48. Analysis of EIS data for common corrosion processes10.1520/STP18062S ↗
49. Structural, electrical, and mechanical properties development during curing of low-k hydrogen silsesquioxane films10.1149/1.1447225 ↗
50. The structural transformation and properties of spin-on poly(silsesquioxane) films by thermal curing10.1016/S0022-3093(02)01373-X ↗
51. Electrical measurements in the study of immersed paint coatings on metal. 1. comparison between capacitance and gravimetric methods of estimating water-uptake10.1002/jctb.5010040202 ↗
52. An impedance model for the estimation of water absorption in organic coatings. Part I: a linear dielectric mixture equation10.1016/S0010-938X(03)00014-3 ↗
53. Theory of dielectric properties of heterogeneous substances applied to water in a paint film10.5006/1.3581974 ↗
54. Metastable pitting of stainless steel10.5006/1.3583880 ↗
55. Metastable pitting corrosion of stainless steel and the transition to stability10.1098/rsta.1992.0114 ↗
56. Dissolution of thin SiO2-coatings –Characterization and evaluation10.1016/j.jnoncrysol.2009.11.003 ↗
57. Dissolution behaviors and applications of silicon oxides and nitrides in transient electronics10.1002/adfm.201304293 ↗
58. Hyrdolysis and condensation of silicon alkoxides
59. Infrared spectroscopy of sol-gel derived silica-based films: a spectra-microstructure overview10.1016/S0022-3093(02)01637-X ↗
60. Ring-opening vibrations of spherosiloxanes10.1021/jp952198t ↗
61. IR spectroscopic investigation of SiO2 film structure10.1016/0040-6090(92)90278-J ↗
62. Electron-beam exposure mechanisms in hydrogen silsesquioxane investigated by vibrational spectroscopy and in situ electron-beam-induced desorption10.1116/1.3425632 ↗
63. Correcting attenuated total reflection − fourier transform infrared spectra for water vapor and carbon dioxide10.1366/000370206778397371 ↗
64. 2.4.3. IR-Raman investigations of gel dehydroxylation