Hydrogen detection in high strength dual phase steel using scanning Kelvin probe technique and XPS analyses
Source abstract
Abstract
Hydrogen permeation through high strength DP1180 steel was studied by Scanning Kelvin Probe (SKP) and X-ray photoelectron spectroscopy (XPS). The XPS analyses showed that hydrogen desorption from the steel increased the ratio Fe(II)/Fe(III) related to oxide film reduction. In parallel, a drop of the electrochemical potential in the oxide film was measured by SKP. Analyses of the composition and potential of the surface were correlated based on Nernst red-ox thermodynamic equilibrium. From this approach, it was shown that the SKP potential can be a measure of hydrogen affecting the surface oxide, but additional contributions should be considered.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Hydrogen embrittlement and corrosion behaviors in metals · Corrosion Behavior and Inhibition · High-Temperature Coating Behaviors
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (59)
Show source-provided references
1. S. Keeler, M. Kimchi, P. J. Mooney, Advanced High-Strength Steels Application Guidelines Version 6.0, (2017) 314.
2. Hydrogen entry and its effect on delayed fracture susceptibility of high strength steel bolts under atmospheric corrosion10.2355/isijinternational.52.267 ↗
3. Hydrogen embrittlement assessment of ultra-high strength steel10.1016/j.corsci.2013.08.013 ↗
4. H. Mohrbacher , Delayed cracking in ultra-high strength automotive steels: damage mechanisms and remedies by microstructural engineering Mater. Sci. Technol. Conf. 2008 1744 1755.
5. Effects of hydrogen on the properties of iron and steel10.1007/BF02654700 ↗
6. Hydrogen damage
7. C. Bergmann, K. Mraczek, B. Kröger, T. Sturel, J. Jürgensen, Y. Yagodzinskyy, X. Guo, F. Vucko, M. Kuhlmann, S. Veith, M. Pohl, Hydrogen embrittlement resistance evaluation of advanced high strength steels in automotive applications, in: SteelyHydrogen, Ghent, Belgium, 2018.
8. Diffusible hydrogen behavior and delayed fracture of cold rolled martensitic steel in consideration of automotive manufacturing process and vehicle service environment10.1016/j.jmrt.2020.09.113 ↗
9. Absorption and diffusion of hydrogen in steels
10. Scanning Kelvin Probe for detection of the hydrogen induced by atmospheric corrosion of ultra-high strength steel10.1016/j.electacta.2016.08.122 ↗
11. Evaluation of hydrogen entry into high strength steel under atmospheric corrosion10.1016/j.corsci.2009.11.046 ↗
12. Evaluation of hydrogen absorption into steel in automobile moving environments10.1016/j.corsci.2015.05.049 ↗
13. Hydrogen thermal desorption relevant to delayed-fracture susceptibility of high-strength steels10.1007/s11661-001-0265-9 ↗
14. Hydrogen trapping phenomena in carbon steel10.1007/BF00540409 ↗
15. A. Nazarov, D. Thierry, Corrosion and hydrogen entry into high strength steel. In situ SKP imaging of the hydrogen flux., in: 65th Annu. Meet. Int. Soc. Electrochem., Lausanne, Switzerland, 2014.
16. Hydrogen entry into Fe and high strength steels under simulated atmospheric corrosion10.1016/j.electacta.2010.09.043 ↗
17. Hydrogen entry behavior into iron and steels under atmospheric corrosion10.2355/tetsutohagane.99.651 ↗
18. Effect of environmental factors on hydrogen absorption into steel sheet under a wet-dry cyclic corrosion condition10.2355/isijinternational.ISIJINT-2020-561 ↗
19. Comparison of corrosion-resistance and hydrogen permeation properties of Zn–Ni, Zn–Ni–Cd and Cd coatings on low-carbon steel10.1016/S0010-938X(02)00228-7 ↗
20. Suitability of Various Materials for Probes in Scanning Kelvin Probe Measurements
21. Hydrogen detection in metals: a review and introduction of a Kelvin probe approach10.1088/1468-6996/14/1/014201 ↗
22. Application of Scanning Kelvin Probe in the study of protective paints10.3389/fmats.2019.00192 ↗
23. Scanning Kelvin Probe as a highly sensitive tool for detecting hydrogen permeation with high local resolution10.1016/j.elecom.2011.10.014 ↗
24. The hydrogen electrode in the dry: a Kelvin probe approach to measuring hydrogen in metals10.1016/j.elecom.2012.08.019 ↗
25. Spatially resolved high sensitive measurement of hydrogen permeation by scanning Kelvin probe microscopy10.1016/j.electacta.2013.04.171 ↗
26. Surface oxide reduction by hydrogen permeation through iron foil detected using a scanning Kelvin probe10.1016/j.elecom.2012.11.022 ↗
27. Measurement of effective hydrogen diffusivity using the Scanning Kelvin Probe10.1016/j.elecom.2013.12.025 ↗
28. Influence of atmospheric oxygen on hydrogen detection on Pd using Kelvin probe technique10.1007/s10008-017-3715-z ↗
29. Challenges in hydrogen quantification using Kelvin probe technique at different levels of relative humidity10.1007/s10008-017-3541-3 ↗
30. Changes on iron electrode surface during hydrogen permeation in borate buffer solution10.1016/j.electacta.2007.11.077 ↗
31. Long‐term atmospheric oxidation of high purity iron10.1149/1.2114007 ↗
32. The oxidation of iron at room temperature10.1016/S0010-938X(65)90096-X ↗
33. Studies of the oxidation of iron by air after being exposed to water vapour using angle-resolved x-ray photoelectron spectroscopy and QUASES10.1002/sia.1992 ↗
34. The mechanism of spontaneous dissolution of the air-formed oxide film on iron in a deaerated neutral phosphate solution10.1016/0376-4583(85)90076-7 ↗
35. XPS study of oxides formed on the surface of high‐purity iron exposed to air - Suzuki - 2000 - surface and interface analysis - wiley online library10.1002/1096-9918(200008)30:1<372::AID-SIA721>3.0.CO;2-R ↗
36. XPS depth profiling study on the passive oxide film of carbon steel in saturated calcium hydroxide solution and the effect of chloride on the film properties10.1016/j.apsusc.2010.12.120 ↗
37. The influence of strain on the passive behavior of carbon steel in cement extract10.1016/j.corsci.2012.08.060 ↗
38. Investigation of multiplet splitting of Fe 2p XPS spectra and bonding in iron compounds10.1002/sia.1984 ↗
39. XPS study of Fe(II)-Fe(III) (oxy)hydroxycarbonate green rust compounds10.1002/sia.2758 ↗
40. Effect of tensile stress on the passivity breakdown and repassivation of AISI 304 stainless steel: a scanning Kelvin probe and scanning electrochemical microscopy study10.1149/2.0251911jes ↗
41. Scanning Kelvin Probe investigation of high-strength steel surface after impact of hydrogen and tensile strain10.3390/cmd1010009 ↗
42. Influence of oxygen and argon plasma treatments on the chemical structure and redox state of oxide covered iron10.1016/S0169-4332(98)00617-5 ↗
43. SKP as a tool to study the physicochemical interaction at buried metal-coating interfaces10.1002/sia.3512 ↗
44. Effect of tensile stress on the passivity breakdown and repassivation of AISI 304 stainless steel: a scanning Kelvin probe and scanning electrochemical microscopy study10.1149/2.0251911jes ↗
45. Analysis of XPS spectra of Fe2+ and Fe3+ ions in oxide materials10.1016/j.apsusc.2007.09.063 ↗
46. Hydrogen concentration in dual-phase (DP) and quenched and partitioned (Q&P) advanced high-strength steels (AHSS) under simulated service conditions compared with cathodic charging conditions10.1002/adem.201600217 ↗
47. Fractographic analysis of the role of hydrogen diffusion on the hydrogen embrittlement susceptibility of DP steel10.1016/j.msea.2015.09.124 ↗
48. Hydrogen trapping in some advanced high strength steels10.1016/j.corsci.2016.05.046 ↗
49. Interactions of CO2 and CO at fractional atmosphere pressures with iron and iron oxide surfaces: one possible mechanism for surface contamination?10.1002/sia.1188 ↗
50. An XPS characterization of FeCO3 films from CO2 corrosion10.1016/S0010-938X(98)00180-2 ↗
51. Organic adlayer on inorganic materials: XPS analysis selectivity to cope with adventitious contamination10.1016/j.apsusc.2016.04.147 ↗
52. Initial oxidation of polycrystalline permalloy surface10.1016/j.susc.2008.07.012 ↗
53. Examination of the oxidation of iron by oxygen using X-ray photoelectron spectroscopy and QUASES10.1016/j.susc.2004.06.210 ↗
54. Change of structure of ferrous oxide at low temperature10.1107/S0365110X53002441 ↗
55. Detection of hydrogen ingress into iron oxide and iron oxy-hydroxide layers by the Kelvin Probe
56. Influence of mechanical stress on the potential distribution on a 301 LN Stainless Steel Surface10.1149/2.0511509jes ↗
57. Effect of hydrogen on electronic structure of fcc iron in relation to hydrogen embrittlement of austenitic steels
58. On a correlation between the hydrogen effects on atomic interactions and mobility of grain boundaries in the alpha-iron. stage i. a change in the electron structure of the alpha-iron due to hydrogen10.1016/j.matlet.2019.126801 ↗
59. Adaptation of the electrochemical permeation technique for studying entry, transport and trapping of hydrogen in metals10.1016/j.electacta.2005.02.151 ↗