journal article·2024-11Open access

Microstructural strain localisation phenomena in fibre-reinforced polymer composites: Insights from nanoscale digital image correlation and finite element modelling

E. Van Vlierberghe, S.F. Gayot, N. Klavzer, C. Breite, T. Pardoen, Y. Swolfs

Abstract

Multiscale models for fibre-reinforced polymer composites currently lack experimentally validated microscale damage descriptors as input parameters. This work demonstrates the occurrence of strain localisation phenomena at the fibre/matrix level using nanoscale digital image correlation. Unidirectional carbon-fibre reinforced epoxy and glass-fibre reinforced PMMA composites were loaded in transverse compression in a scanning electron microscope. Radial and shear strain maps were extracted and compared with finite element simulations based on a conventional elastoplastic model. Near the interface, an interphase layer is present in the matrix, presumably due to locally different polymerisation conditions. A skin-core structure was found in carbon fibres, corresponding to an increased transverse modulus towards the interface.
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Research context

OpenAlex topics: Optical measurement and interference techniques · Mechanical Behavior of Composites · Advanced machining processes and optimization

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References (45)

Show source-provided references
1. Multiscale modeling of composites: toward virtual testing ⋯ and beyond10.1007/s11837-012-0509-8 ↗
2. Multiscale modeling of composite materials: a roadmap towards virtual testing10.1002/adma.201101683 ↗
3. Nanomechanics serving polymer-based composite research
4. Multi-scale characterization and modelling of the transverse compression response of unidirectional carbon fiber reinforced epoxy10.1016/j.compstruct.2018.10.076 ↗
5. Nanoindentation of neat and in situ polymers in polymer-matrix composites10.1016/j.compscitech.2004.09.001 ↗
6. Fibrous composite matrix characterisation using nanoindentation: the effect of fibre constraint and the evolution from bulk to in-situ matrix properties10.1016/j.compositesa.2014.09.022 ↗
7. Experimental determination of the true epoxy resin strength using micro-scaled specimens10.1016/j.compositesa.2006.08.006 ↗
8. Experimental characterization of tensile properties of epoxy resin by using micro-fiber specimens10.1177/0731684416669248 ↗
9. Extreme scale-dependent tensile properties of epoxy fibers10.3144/expresspolymlett.2019.86 ↗
10. In-situ observations of microscale ductility in a quasi-brittle bulk scale epoxy10.3390/polym12112581 ↗
11. The glass fiber-polymer matrix interface/interphase characterized by nanoscale imaging techniques10.1016/j.compscitech.2013.04.014 ↗
12. Determining the interphase thickness and properties in polymer matrix composites using phase imaging atomic force microscopy and nanoindentation10.1163/156856100743248 ↗
13. Electron-microscope studies of structural heterogeneity in pan-based carbon fibres10.1016/0008-6223(79)90067-8 ↗
14. Structural heterogeneity and stress distribution in carbon fiber monofilament as revealed by synchrotron micro-beam X-ray scattering and micro-Raman spectral measurements10.1016/j.carbon.2010.12.048 ↗
15. Texture of PAN- and pitch-based carbon fibers10.1016/S0008-6223(01)00139-7 ↗
16. Direct observation of nanocrystallite buckling in carbon fibers under bending load10.1103/PhysRevLett.95.225501 ↗
17. Stress-induced microstructural changes and crystallite modulus of carbon fiber as measured by X-ray scattering10.1016/j.carbon.2011.10.029 ↗
18. Stress concentration in carbon fiber revealed by the quantitative analysis of X-ray crystallite modulus and Raman peak shift evaluated for the variously-treated monofilaments under constant tensile forces10.1016/j.carbon.2012.10.012 ↗
19. Characterization of the interphase in carbon fiber/polymer composites using a nanoscale dynamic mechanical imaging technique10.1016/j.carbon.2010.05.008 ↗
20. Nanoscale dynamic mechanical imaging of the skin–core difference: from PAN precursors to carbon fibers10.1016/j.matlet.2014.04.176 ↗
21. Modulus distribution in polyacrylonitrile-based carbon fiber monofilaments10.1016/j.carbon.2019.09.084 ↗
22. Determination of transverse and shear moduli of single carbon fibres10.1016/j.carbon.2019.11.054 ↗
23. Application of digital image correlation at the microscale in fiber-reinforced composites10.1016/j.compositesa.2011.07.014 ↗
24. Full-field strain measurements at the micro-scale in fiber-reinforced composites using digital image correlation10.1016/j.compstruct.2015.12.020 ↗
25. Strain mapping at the micro-scale in hierarchical polymer composites with aligned carbon nanotube grafted fibers10.1016/j.compscitech.2016.10.021 ↗
26. One-step deposition of nano-to-micron-scalable, high-quality digital image correlation patterns for high-strain in-situ multi-microscopy testing10.1111/str.12330 ↗
27. Nanoscale digital image correlation at elementary fibre/matrix level in polymer–based composites10.1016/j.compositesa.2023.107455 ↗
28. Development of a versatile speckle pattern of nano-sized polymer particles for high-resolution SEM-DIC10.1016/j.polymertesting.2023.108134 ↗
29. Ncorr: open-source 2D digital image correlation matlab software10.1007/s11340-015-0009-1 ↗
30. In-situ full field out of plane displacement and strain measurements at the micro-scale in single reinforcement composites under transverse load10.1007/s11340-019-00541-z ↗
31. Mechanical characterization and modeling of the deformation and failure of the highly crosslinked RTM6 epoxy resin10.1007/s11043-016-9336-6 ↗
32. Maes · 2020
33. Stress concentrations in an impregnated fibre bundle with random fibre packing10.1016/j.compscitech.2012.10.013 ↗
34. Gayot · 2023
35. Longitudinal debonding in unidirectional fibre-reinforced composites: numerical analysis of the effect of interfacial properties
36. Van Vlierberghe
37. Influence of physical ageing and fibre proximity on the local mechanical response of the Elium® thermoplastic composite matrix10.1016/j.compositesa.2024.108141 ↗
38. Evolution of effective mechanical and interphase properties during natural ageing of glass-fibre/epoxy composites using micromechanical approach10.1016/j.compstruct.2020.113399 ↗
39. An integrated computational materials engineering framework to analyze the failure behaviors of carbon fiber reinforced polymer composites for lightweight vehicle applications10.1016/j.compscitech.2020.108560 ↗
40. A micromechanical study of residual stress and its effect on transverse failure in polymer–matrix composites10.1016/j.ijsolstr.2005.08.012 ↗
41. A numerical micro-mechanical study on damage induced by the curing process in carbon/epoxy unidirectional material10.1016/j.compstruct.2018.11.059 ↗
42. Transverse compression failure of unidirectional composites10.1002/pc.22996 ↗
43. Micromechanical analysis of polymer composites reinforced by unidirectional fibres: Part II – micromechanical analyses10.1016/j.ijsolstr.2013.02.007 ↗
44. A microscopic elasto-plastic damage model for characterizing transverse responses of unidirectional fiber-reinforced polymer composites10.1016/j.tws.2020.106828 ↗
45. Discovering plasticity models without stress data10.1038/s41524-022-00752-4 ↗