journal article·2017Open access

Fabrication of dense Si3N4 ceramics via coating amorphous Si3N4 nano-powders by sodium reduction in liquid ammonia

Qi WANG, Mei YANG, Jiusan XIAO, Hongmin ZHU

Abstract

Commercial Si3N4 powders coated with 0–30% amorphous Si3N4 nano-powders were fabricated successfully. Amorphous Si3N4 nano-powders coating were prepared through the reduction of silicon tetrachloride (SiCl4) by sodium in liquid ammonia at −45°C. Dense Si3N4 ceramics with 97.2% relative density of theoretic value were obtained from Si3N4 micro-powders coated with 30% nano-powders sintered by spark plasma sintering at 1500°C without sintering additives.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Nuclear materials and radiation effects

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing

State Key Laboratory of Biochemical Engineering, Institute of Process Engineering Chinese Academy of Sciences

Department of Metallurgy, Graduate School of Engineering, Tohoku University

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