journal article·2013-09Open access

Synthesis of silica–titania composite oxide via “green” aqueous peroxo-route

I. V. Krivtsov, M. V. Ilkaeva, V. D. Samokhina, V. V. Avdin, S. A. Khainakov, D. A. Uchaev, J. R. Garcia

Abstract

The preparation procedure of silica–titania composite oxide using novel solution/sol single precursor containing titanium peroxocomplex and silicic acid has been described. Pechini-type sol–gel process has been used to prepare oxides from the aqueous precursor. Some structural, morphological and textural characteristics of the prepared material have been presented. Composite SiO2/TiO2 has high surface area (c.a. 300 m2/g), and it is composed of anatase nanoparticles with the mean diameter of 5 nm embedded in amorphous silica, then TiO2 prepared via similar method is presented as a mixture of anatase and rutile phases. The proposed synthetic procedure meets the requirements of “green chemistry”.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: TiO2 Photocatalysis and Solar Cells · Polyoxometalates: Synthesis and Applications · Catalytic Processes in Materials Science

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