journal article·2024-01-11Open access

A Comparison of 90° Bending for Foldable Electronics

Megan J. Cordill, Patrice Kreiml, Harald Köstenbauer, Christian Mitterer

Coatings· Volume 14· Issue 1

Abstract

In order to assess the longevity of foldable electronics, folding or bending tests on model systems need to be performed. However, not all bending tests are created equal in that different configurations lead to different amounts of mechanical damage and thus different electrical responses. Two 90° bending instruments were compared using two model metallic thin film systems on polyimide to establish if the two seemingly similar bending tests yield the same results. The two film systems, namely 300 nm Mo and 130 nm Al on 50 nm Mo, were magnetron-sputtered on polyimide substrates and tested in the custom-built FLEX-E-TEST and the commercially available YUASA test that is capable of in situ resistance measurements. For statistics, 10–12 samples were tested of each film system on each folding device using the same applied bending strain and number of cycles. Samples were intermittently characterized with confocal laser scanning microscopy and electrical resistance to correlate the amount of mechanical damage (crack density) with the electrical normalized resistance ratio of the damaged area. The results show that even with the same bending radius, a similar but not identical amount of mechanical damage forms for both bending devices. Additionally, the resistance as a function of cycles also differs after 10,000 cycles. A closer examination of the damage, especially in the Al/Mo film system, indicates that the speed of the bending, and if the samples experience spring back, can alter the received mechanical damage. The in situ resistance data of the YUASA test were further examined and a suggestion of standardizing how folding or bending test results are reported is provided.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Advanced Sensor and Energy Harvesting Materials · Electronic Packaging and Soldering Technologies · Advanced Materials and Mechanics

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Erich Schmid Institute of Materials Science, Austrian Academy of Sciences, 8700 Leoben, Austria

Business Division Electronics, Plansee SE, 6600 Reutte, Austria

Department of Materials Science, Montanuniversität Leoben, 8700 Leoben, Austria

Funding

Austrian Research Promotion Agency (FFG)

References (35)

Show source-provided references
1. Saleh, R., Barth, M., Eberhardt, W., and Zimmermann, A. (2021). Bending Setups for Reliability Investigation of Flexible Electronics. Micromachines, 12.10.3390/mi12010078 ↗
2. The Effect of Bending Loading Conditions on the Reliability of Inkjet Printed and Evaporated Silver Metallization on Polymer Substrates10.1016/j.microrel.2015.10.007 ↗
3. Effect of Film Thickness on the Stretchability and Fatigue Resistance of Cu Films on Polymer Substrates10.1557/jmr.2014.339 ↗
4. A Four-Point Bending Technique for Studying Subcritical Crack Growth in Thin Films and at Interfaces10.1557/JMR.1997.0122 ↗
5. Mechanical and Environmental Durability of Roll-to-Roll Printed Silver Nanoparticle Film Using a Rapid Laser Annealing Process for Flexible Electronics10.1016/j.microrel.2014.07.004 ↗
6. Theoretical and Experimental Studies of Bending of Inorganic Electronic Materials on Plastic Substrates10.1002/adfm.200800306 ↗
7. Experimental and Analytical Studies on the High Cycle Fatigue of Thin Film Metal on PET Substrate for Flexible Electronics Applications10.1109/TCPMT.2010.2100911 ↗
8. Mechanical and Electrical Properties of Ultra-Thin Chips and Flexible Electronics Assemblies during Bending10.1016/j.microrel.2014.07.125 ↗
9. Reliability of OTFTs on Flexible Substrate: Mechanical Stress Effect10.1051/epjap/2011100426 ↗
10. Transition from Dislocation Glide to Creep Controlled Damage in Fatigued Thin Cu Films10.1063/1.4819760 ↗
11. Experimental Study on Buckle Evolution of Thin Inorganic Layers on a Polymer Substrate10.1016/j.engfracmech.2010.07.012 ↗
12. Effects of Bending Fatigue on the Electrical Resistance in Metallic Films on Flexible Substrates10.1007/s12540-010-1213-2 ↗
13. Mechanical Analyses and Structural Design Requirements for Flexible Energy Storage Devices10.1002/aenm.201700535 ↗
14. Measurement of the Ultimate Shear Strength of a Metal-Ceramic Interface10.1016/0001-6160(89)90120-X ↗
15. Compressive and Tensile Bending of Sputter Deposited Al/Mo Bilayers10.1016/j.scriptamat.2018.11.048 ↗
16. Size Effects in the Fatigue Behavior of Thin Ag Films10.1016/S1359-6454(02)00391-9 ↗
17. On the Difference of Fatigue Strengths from Rotating Bending, Four-Point Bending, and Cantilever Bending Tests10.1016/S0308-0161(00)00080-6 ↗
18. Mechanical Failure of Brittle Thin Films on Polymers during Bending by Two-Point Rotation10.1016/j.tsf.2016.05.025 ↗
19. Buckle Morphology of Compressed Inorganic Thin Layers on a Polymer Substrate10.1016/j.tsf.2005.11.106 ↗
20. A Multidimensional Scheme of Characterization for Performance Deterioration Behavior of Flexible Devices under Bending Deformation10.1016/j.tsf.2019.137613 ↗
21. Reliability Issues and Solutions in Flexible Electronics Under Mechanical Fatigue10.1007/s13391-018-0043-0 ↗
22. Improving Mechanical Fatigue Resistance by Optimizing the Nanoporous Structure of Inkjet-Printed Ag Electrodes for Flexible Devices10.1088/0957-4484/25/12/125706 ↗
23. Wright, D.N., Vardøy, A.S.B., Belle, B.D., Visser Taklo, M.M., Hagel, O., Xie, L., Danestig, M., and Eriksson, T. (2017, January 18–20). Bending Machine for Testing Reliability of Flexible Electronics. Proceedings of the 2017 IMAPS Nordic Conference on Microelectronics Packaging, NordPac 2017, Gothenburg, Sweden.10.1109/NORDPAC.2017.7993162 ↗
24. Explicit Relationship between Electrical and Topological Degradation of Polymer-Supported Metal Films Subjected to Mechanical Loading10.1063/1.4982802 ↗
25. Cordill, M.J., Kreiml, P., and Mitterer, C. (2022). Materials Engineering for Flexible Metallic Thin Film Applications. Materials, 15.10.3390/ma15030926 ↗
26. Metal Films on Polymer Substrates Stretched beyond 50%10.1063/1.2817234 ↗
27. Correlation of Mechanical Damage and Electrical Behavior of Al/Mo Bilayers Subjected to Bending10.1016/j.tsf.2019.137480 ↗
28. Linking Through-Thickness Cracks in Metallic Thin Films to in-Situ Electrical Resistance Peak Broadening10.1016/j.scriptamat.2022.114550 ↗
29. Role of Layer Order on the Equi-Biaxial Behavior of Al/Mo Bilayers10.1016/j.scriptamat.2020.113656 ↗
30. The Sputter Performance of an Industrial-Scale Planar Mo-Target over Its Lifetime: Target Erosion and Fi Lm Properties10.1016/j.surfcoat.2019.125174 ↗
31. Fatigue of Polymer-Supported Ag Thin Films10.1016/j.scriptamat.2012.02.030 ↗
32. Effects of Stretching and Cycling on the Fatigue Behavior of Polymer-Supported Ag Thin Films10.1016/j.msea.2013.03.043 ↗
33. Improved Electro-Mechanical Reliability of Flexible Systems with Alloyed Mo-Ta Adhesion Layers10.1016/j.tsf.2021.138533 ↗
34. Improving the Stretchability of As-Deposited Ag Coatings on Poly-Ethylene-Terephthalate Substrates through Use of an Acrylic Primer10.1063/1.3567917 ↗
35. Relationship between Mechanical Damage and Electrical Degradation in Polymer-Supported Metal Films Subjected to Cyclic Loading10.1016/j.msea.2016.03.052 ↗