journal article·2023-01-30Open access

Optimization of Electropolishing Process Using Taguchi Robust Design for UNS N08367 in a Mixed Solution of Sulfuric Acid and Phosphoric Acid

Hyun-Kyu Hwang, Seong-Jong Kim

Coatings· Volume 13· Issue 2

Abstract

The purpose of this investigation was to determine the optimal conditions for UNS N08367 electropolishing using the Taguchi method. The investigated factors were the electrolyte composition ratio, applied current density, and electrolyte temperature. Each factor was tested at three levels. Electropolishing was optimized using analysis of variance (ANOVA), signal-to-noise ratio (the smaller the better the characteristics), and surface analysis. The ANOVA results showed that among the three factors, only the electrolyte composition ratio was effective in surface planarization. The optimal conditions for electropolishing determined according to the signal-to-noise ratio were a sulfuric acid-to-phosphoric acid ratio of 2:8, a current density of 400 mA/cm2, and an electrolyte temperature of 75 °C.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Advanced Machining and Optimization Techniques · Nanofabrication and Lithography Techniques · Anodic Oxide Films and Nanostructures

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Graduate School, Mokpo National Maritime University, 91, Haeyangdaehak-ro, Mokpo-si 58628, Republic of Korea

Division of Marine Engineering, Mokpo National Maritime University, 91, Haeyangdaehak-ro, Mokpo-si 58628, Republic of Korea

Funding

Ministry of Oceans and Fisheries · Ministry of Oceans and Fisheries, Korea

References (38)

Show source-provided references
1. Machining Characteristics of the electropolishing of stainless steel (STS316L)10.1007/s001700070049 ↗
2. A Study of Micro Electrolytic-deburring for Nitinol
3. A Study on the Characteristics of Micro Electropolishing for Stainless Steel10.1007/s00170-015-8041-y ↗
4. Effect of Grain Size on Corrosion Resistance and High Temperature Oxidation Behavior of 22Cr-12Ni-5W Super Austenitic Stainless Steels
5. Microsegregation-related pitting corrosion characteristics of AL-6XN superaustenitic stainless steel laser welds10.1016/j.corsci.2010.07.007 ↗
6. Pitting corrosion resistance of austenitic and superaustenitic stainless steels in aqueous medium of NaCl and H2SO410.1557/jmr.2016.198 ↗
7. Experiment Investigation for Design on the Sensitization-Dependent Passivation Characteristics of AL-6XN in 3.5% NaCl Solution10.1166/jnn.2021.19219 ↗
8. Mahardika, M., Setyawan, M.A., Sriani, T., Miki, N., and Prihandana, G.S. (2021). Electropolishing Parametric Optimization of Surface Quality for the Fabrication of a Titanium Microchannel Using the Taguchi Method. Machines, 9.10.3390/machines9120325 ↗
9. Taguchi Design of Experiment for the Optimization of Electrochemical Polishing of Metal Additive Manufacturing Components
10. Comparative XPS analyses of passive layers composition formed on Duplex 2205 SS after standard and high-current-density electropolishing
11. The optimal parameters in a magnetically assisted finishing system using Taguchi’s method10.1016/j.physb.2010.08.017 ↗
12. Effect of Seawater Temperature on the Cyclic Potentiodynamic Polarization Characteristics and Microscopic Analysis on Damage Behavior of Super Austenitic Stainless Steel
13. (2018). Standard No. ASTM B912.
14. Design Optimization of Earth Retaining Walls Using the Taguchi Method
15. Electropolishing of 304 stainless steel: Surface roughness control using experimental design strategies and a summarized electropolishing model10.1016/j.electacta.2007.11.075 ↗
16. Roughness Reduction of Additively Manufactured Steel by Electropolishing10.1007/s00170-019-04720-z ↗
17. Electropolishing of Re-melted SLM Stainless Steel 316L Parts Using Deep Eutectic Solvents: 3 × 3 Full Factorial Design10.1007/s11665-016-2140-2 ↗
18. Electropolishing of surfaces: Theory and applications10.1080/02670844.2016.1198452 ↗
19. Design of Experiments: Useful Orthogonal Arrays for Number of Experiments from 4 to 1610.3390/e9040198 ↗
20. Lee, S.B. (2018). Minitab Example-driven Design of Experiments, ERETECH.
21. Experimental investigation of selective laser melting parameters for higher surface quality and microhardness properties: Taguchi and super ranking concept approaches
22. An Overview of the Strategy and Tactics of Taguchi10.1080/07408178808966177 ↗
23. An overview of Taguchi method and newly developed statistical methods for robust design10.1080/07408179208964244 ↗
24. Yang, B.T. (2011). Optimal Design of the Flux Barrier in the Spoke Type BLDC Motor Using the Modified Taguchi Method. [Ph.D. Thesis, The Graduate School of Industry Hanyang University].
25. Taguchi, G. (1986). Introduction to Quality Engineering: Designing Quality into Products and Processes, Quality Resources, American, Asian Productivity Organization.
26. Freddi, A., and Salmon, M. (2019). Design Principles and Methodologies, Springer. Chapter 9.10.1007/978-3-319-95342-7 ↗
27. Prediction of Pitting Corrosion Characteristics of AL-6XN Steel with Sensitization and Environmental Variables Using Multiple Linear Regression Method
28. Fundamental aspects and applications of electrochemical microfabrication10.1016/S0013-4686(00)00350-9 ↗
29. Understanding Effect Sizes10.7599/hmr.2015.35.1.40 ↗
30. Standardized or simple effect size: What should be reported?10.1348/000712608X377117 ↗
31. H Electropolishing Characteristics of Stainless Steel for Industrial Application10.5695/JKISE.2016.49.4.363 ↗
32. Optimum reference temperature for reparameterization of the Arrhenius equation. Part 1: Problems involving one kinetic constant10.1016/j.ces.2007.02.020 ↗
33. Pitting and crevice corrosion behaviour of superaustenitic stainless steels in sea water cooling systems10.1515/CORRREV.2000.18.6.429 ↗
34. Electrochemical Characteristics of Superaustenitic Stainless Steel with Temperature in Sea Water
35. Electrochemical Properties of Austenitic Stainless Steel with Initial Delay Time and Surface Roughness in Electropolishing Solution
36. Kim, S.H. (2016). Process Optimization for Life Extension of Electropolishing Solution for Semiconductor Piping Tube. [Ph.D. Thesis, Kwangwoon University].
37. Science and Industry of Electropolishing
38. Electropolishing of 316L stainless steel for anticorrosion passivation10.1361/105994901770344827 ↗