Preparation and Characterization of the Cr-Nanodiamonds/MoN Coatings with Performant Mechanical Properties
Source abstract
Abstract
This paper presents the results of a study on the preparation and characterization of a Cr-DND/MoN detonation chromium-nanodiamond coating deposited on cemented tungsten carbide (WC–3 wt.% Co) mill blades using Arc-PVD and electrodeposition methods. The physical and mechanical characteristics of the coatings were investigated by scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), XRD analysis, Raman spectroscopy, micro-identification, and scratch test (evaluation of the coating adhesion). It was shown that the Cr-DND/MoN coating consists of successive layers of Cr-DND (top), Cu (middle) and MoN (bottom) with separate phases of γ-Mo2N, α-Mo, α-Cu, Cr-DND and nanodiamonds. The Cr-DND composite electrochemical coating (CEC) was deposited from the conventional chromium plating electrolyte with the addition of nanodiamonds. The copper interlayer was deposited by the Arc-PVD method on the surface of the MoN coating to improve the adhesion strength of the Cr-DND CEC. The coating showed an optimum microhardness of about 14 ± 1 GPa and good adhesion with a critical load Lc of about 93 N. In addition to the expected experimental results, the coating has high wear resistance, confirmed by scratch tests.
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Research context
OpenAlex topics: Advanced materials and composites · Diamond and Carbon-based Materials Research · Metal and Thin Film Mechanics
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Department of Physics, Faculty of Information Technology, Belarusian State Technological University, 13a, Sverdlov Street, 220006 Minsk, Belarus
Chimie ParisTech, PSL University, CNRS, IRCP, 75005 Paris, France
Sorbonne Université, 4 Place Jussieu, 75231 Paris, France
Department of Chemistry, Technology of Electrochemical Production and Electronic Engineering Materials, Chemical Technology and Engineering Faculty, Belarusian State Technological University, 13a, Sverdlov Street, 220006 Minsk, Belarus
Department of Solid State Physics, Faculty of Physics, Belarusian State University, 4, Nezavisimosti Avenue, 220030 Minsk, Belarus
The Joint Institute of Mechanical Engineering of the NAS of Belarus, 12, Akademicheskaya Street, 220072 Minsk, Belarus
Funding
State Budget Program of Science Researches of the Republic of Belarus
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