journal article·2021-06-16Open access

Influence of Alternative and Conventional Surface Treatments on the Bonding Mechanism between PEEK and Veneering Resin for Dental Application

Regina F. Villefort, Lilian C. Anami, Tiago M. B. Campos, Renata M. Melo, Luiz F. Valandro, Sandra L. V. von Zeidler, Marco A. Bottino

Coatings· Volume 11· Issue 6

Abstract

This study evaluated the influence of conventional and alternative surface treatments on wettability and the bond strength between polyether ether ketone (PEEK) and veneering resin. PEEK samples were randomly divided into five groups: sandblasting, tribochemical silica coating, etching with 98% sulfuric acid for 5 s, etching with 98% sulfuric acid for 30 s, and tribochemical silica coating plus heated silane. One of them was subjected to analysis by energy-dispersive X-ray spectroscopy (EDS) and ten were analyzed by goniometry (n = 5) and scanning electron microscopy (n = 5). Shear bond strength (SBS) was tested, and failure types were assessed. Data were analyzed using one-way ANOVA, followed by the Tukey and Duncan tests (all, α = 5%). Treatment with sandblasting and silica coating had the lowest SBS means (4.2 MPa and 4.4 MPa respectively), while sulfuric acid for 5 s showed the highest mean value (12.6 MPa), followed by sulfuric acid for 30 s and tribochemical + heated silane. All failures were classified as adhesive. The lowest mean contact angle was found for the polished (control) and etched group with 98% sulfuric acid for 30 s (83.9°). Etching with 98% sulfuric acid for 5 s increased the SBS between resin and PEEK.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Dental materials and restorations · Endodontics and Root Canal Treatments · Dental Implant Techniques and Outcomes

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Biotechnology Postgraduate Program, Federal University of Espírito Santo (UFES), RENORBIO, 1468 Marechal Campos Avenue, Vitória 29043-900, ES, Brazil

Department of Dental Materials and Prosthodontics, Institute of Science and Technology, São Paulo State University (UNESP), 777 Eng. José Longo Avenue, São José dos Campos 12245-000, SP, Brazil

Physics Department, Aeronautics Institute of Technology (ITA), 50 Marechal Eduardo Gomes Square, São José dos Campos 12228-900, SP, Brazil

MSc-PhD Post-Graduate Program in Oral Science (Prosthodontic Unit), Faculty of Odontology, Federal University of Santa Maria (UFSM), 1184 Marechal Floriano Peixoto Street, Santa Maria 97015-372, RS, Brazil

Funding

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior · Fundação de Amparo à Pesquisa e Inovação do Espírito Santo

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