journal article·2019-12-09Open access

Non-Evaporable Getter Ti-V-Hf-Zr Film Coating on Laser-Treated Aluminum Alloy Substrate for Electron Cloud Mitigation

Jie Wang, Yong Gao, Zhiming You, Jiakun Fan, Jing Zhang, Zhaopeng Qiao, Sheng Wang, Zhanglian Xu

Coatings· Volume 9· Issue 12

Abstract

For improving the vacuum and mitigating the electron clouds in ultra-high vacuum chamber systems of high-energy accelerators, the deposition of Ti-V-Hf-Zr getter film on a laser-treated aluminum alloy substrate was proposed and exploited for the first time in this study. The laser-treated aluminum surface exhibits a low secondary electron yield (SEY), which is even lower than 1 for some selected laser parameters. Non-evaporable getter (NEG) Ti-V-Hf-Zr film coatings were prepared using the direct current (DC) sputtering method. The surface morphology, surface roughness and composition of Ti-V-Hf-Zr getter films were characterized and analyzed. The maximum SEY of unactivated Ti-V-Hf-Zr getter film on laser-treated aluminum alloy substrates ranged from 1.10 to 1.48. The X-ray photoelectron spectroscopy (XPS) spectra demonstrate that the Ti-V-Hf-Zr coated laser-treated aluminum alloy could be partially activated after being heated at 100 and 150 °C, respectively, for 1 h in a vacuum and also used as a pump. The results were demonstrated initially and the potential application should be considered in future particle accelerators.
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Research context

OpenAlex topics: Laser-Plasma Interactions and Diagnostics · Plasma Diagnostics and Applications · Electron and X-Ray Spectroscopy Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Shaanxi Engineering Research Center of Advanced Nuclear Energy & Shaanxi Key Laboratory of Advanced Nuclear Energy and Technology & School of Energy and Power Engineering, Xi’an Jiaotong University, Xi’an 710049, China

Funding

Postdoctoral Research Foundation of China · National Natural Science Foundation of China · Fundamental Research Funds for the Central Universities · Shaanxi Province Postdoctoral Science Foundation · key project of Intergovernmental International Scientific and Technological Innovation Cooperation in China

References (43)

Show source-provided references
1. Effect of coating morphology on the electron stimulated desorption from Ti-Zr-Hf-V nonevaporable-getter-coated stainless steel10.1016/j.vacuum.2012.04.033 ↗
2. Pumping properties of Ti-Zr-Hf-V non-evaporable getter coating10.1016/j.vacuum.2013.07.035 ↗
3. Pumping and electron-stimulated desorption properties of a dual-layer nonevaporable getter10.1116/1.4964612 ↗
4. Development of copper electroformed vacuum chambers with integrated nonevaporable getter thin film coatings10.1116/1.4999539 ↗
5. A novel route to extreme vacua: The non-evaporable getter thin film coatings10.1016/S0042-207X(98)00377-7 ↗
6. XPS analysis of the activation process in non-evaporable getter thin films10.1002/1096-9918(200008)30:1<623::AID-SIA719>3.0.CO;2-Y ↗
7. NEG coating deposition and characterisation of narrow-gap insertion devices and small-diameter chambers for light sources and particle accelerators10.1016/j.vacuum.2016.12.036 ↗
8. Achievements and problems in the first commissioning of superKEKB vacuum system10.1116/1.4977764 ↗
9. Rumolo, G., Bartosik, H., Belli, E., Dijkstal, P., Iadarola, G., Li, K., Mether, L., Romano, A., Schenk, M., and Zimmermann, F. (2017, January 14–19). Electron cloud effects at the LHC and LHC injectors. Proceedings of the IPAC 2017, Copenhagen, Denmark.
10. Reduction of secondary electron yield for E-cloud mitigation by laser ablation surface engineering10.1016/j.apsusc.2017.02.013 ↗
11. Experimental study on TiN coated racetrack-type ceramic pipe10.1088/1674-1137/39/11/117005 ↗
12. Effects of TiN film coating on electrochemical behaviours of nanotube formed Ti-xHf alloys10.1016/S1003-6326(08)60364-7 ↗
13. Amorphous carbon coatings for the mitigation of electron cloud in the CERN Super Proton Synchrotron10.1103/PhysRevSTAB.14.071001 ↗
14. Vallgren, C.Y., Chiggiato, P., Pinto, P.C., Neupert, H., Rumolo, G., Shaposhnikova, E., Taborelli, M., and Kato, S. (2011, January 4–9). Performance of carbon coatings for mitigation of electron cloud in the SPS. Proceedings of the IPAC 2011, San Sebastián, Spain.
15. Eldred, J., Backfish, M., Tan, C.Y., Zwaska, R., and Kato, S. (2017, January 14–19). Beam tests of diamond-like carbon coating for mitigation of electron cloud. Proceedings of the IPAC 2017, Copenhagen, Denmark.
16. Secondary electron emission characteristics of graphene films with copper substrate10.1088/1674-1137/40/11/117003 ↗
17. Study on the effect of laser parameters on the SEY of aluminum alloy10.1109/TNS.2019.2898922 ↗
18. Ti 2p and O 1s core levels and chemical bonding in titanium-bearing oxides10.1016/j.elspec.2006.02.004 ↗
19. Change of Ti 2p XPS spectrum for titanium oxide by Ar ion bombardment
20. XPS and ESD study of carbon and oxygen chemistry on TiZrV NEG10.1016/S0042-207X(00)00469-3 ↗
21. XPS and SIMS study of the ageing mechanism of Zr-V non-evaporable getter films10.1016/j.apsusc.2004.05.125 ↗
22. Zirconium dioxide thin films characterized by XPS10.1116/1.1375573 ↗
23. Mechanism of non-evaporable getter activation XPS and static SIMS study of Zr44V56 alloy10.1016/S0042-207X(02)00756-X ↗
24. XPS study of the initial oxidation of the bulk metallic glass Zr46.75Ti8.25Cu7.5Ni10Be27.510.1007/s10853-008-2834-4 ↗
25. Surface oxidation of amorphous Zr65Cu17.5Ni10Al7.5 and Zr46.75Ti8.25Cu7.5Ni10Be27.510.1016/S0921-5093(00)01586-0 ↗
26. As-received, ozone cleaned and Ar+ sputtered surfaces of hafnium oxide grown by atomic layer deposition and studied by XPS10.1116/11.20100601 ↗
27. Hafnium oxide thin film grown by ALD: An XPS study10.1116/11.20080401 ↗
28. The secondary electron yield of technical materials and its variation with surface treatments
29. Grosso, D.R., Commisso, M., Cimino, R., Flammini, R., Larciprete, R., and Wanzenberg, R. (2011, January 4–9). SEY of Al samples from the dipole chamber of PETRA III at DESY. Proceedings of the IPAC 2011, San Sebastián, Spain.
30. Effect of the surface processing on the secondary electron yield of Al alloy samples
31. Carbon coatings with low secondary electron yield10.1016/j.vacuum.2013.03.001 ↗
32. Secondary electron emission under electron bombardment from graphene nanoplatelets10.1016/j.apsusc.2013.10.045 ↗
33. Secondary electron emission on space materials: Evaluation of the total secondary electron yield from surface potential measurements10.1109/TPS.2011.2172636 ↗
34. The controlled preparation of low SEE surfaces by evaporation of metal films under high residual gas pressures10.1088/0022-3727/3/10/312 ↗
35. Influence of air exposures and thermal treatments on the secondary electron yield of copper10.1116/1.582286 ↗
36. James, M.S., Ronald, A.C., Robert, A.L., and Tod, L. (2016, January 25–29). Engineered surfaces to control secondary electron emission for multipactor suppression. Proceedings of the 2016 IEEE National Aerospace and Electronics Conference (NAECON) and Ohio Innovation Summit (OIS), Dayton, OH, USA.
37. Outgassing measurement of an LHC collimator and estimation for the NEG performances10.1016/j.vacuum.2011.03.004 ↗
38. Ion-stimulated gas desorption yields of electropolished, chemically etched, and coated (Au, Ag, Pd, TiZrV) stainless steel vacuum chambers and St707 getter strips irradiated with 4.2 MeV/u lead ions
39. First experimental and simulation study on the secondary electron and photoelectron yield of NEG materials (Ti-Zr-V) coating under intense photon irradiation10.1016/j.nima.2005.08.061 ↗
40. Pimpec, L., King, F., Kirby, R.E., Pivi, M., and Rumolo, G. (2004). The Continuing Story of Secondary Electron Yield Measurements from TiN Coating and TiZrV Getter Film. SLAC-TN-04-046\LCC-0146, Stanford Linear Accelerator Center.
41. Properties of TiN and TiZrV thin film as a remedy against electron cloud10.1016/j.nima.2005.05.048 ↗
42. Vallgren, C.Y., Arduini, G., Bauche, J., Calatroni, S., Chiggiato, P., Cornelis, K., Pinto, P.C., M’etral, E., Rumolo, G., and Shaposhnikova, E. (2010, January 23–28). Amorphous carbon coatings for mitigation of electron cloud in the CERN SPS. Proceedings of the IPAC’10, Kyoto, Japan.
43. The secondary electron yield of TiZr and TiZrV non-evaporable getter thin film coatings10.1016/S0169-4332(00)00838-2 ↗