journal article·2022-10-06Open access

Change in Dimensions and Surface Roughness of 42CrMo4 Steel after Nitridation in Plasma and Gas

David Dobrocky, Zdenek Pokorny, Zdenek Joska, Josef Sedlak, Jan Zouhar, Jozef Majerik, Zbynek Studeny, Jiri Prochazka, Igor Barenyi

Coatings· Volume 12· Issue 10

Abstract

The influence of plasma nitriding and gas nitriding processes on the change of surface roughness and dimensional accuracy of 42CrMo4 steel was investigated in this paper. Both processes almost always led to changes in the surface texture. After plasma nitriding, clusters of nitride ions were formed on the surface of steel, while gas nitriding very often led to the new creation of a formation of a “plate-like” surface texture. In both cases of these processes, a compound layer in specific thickness was formed, although the parameters of the processes were chosen with the aim of suppressing it. After the optimizing of nitriding parameters during nitriding processes, it was found that there were no changes in the surface roughness evaluated using the Ra parameter. However, it turned out that when using a multi-parameter evaluation of roughness (the parameters Rz, Rsk and Rku were used), there were presented some changes in roughness due to nitriding processes, which affect the functional behavior of the components. Roughness changes were also detected by evaluating surface roughness profiles, where nitriding led to changes in peak heights and valley depths. Nitriding processes further led to changes in dimensions in the form of an increase of 0.032 mm on average. However, the magnitude of the change has some context on chemical composition of material. A larger increase in dimensions was found with gas nitriding. The change in the degree of IT accuracy is closely related to the change in dimension. For both processes, there was a change of one degree of IT accuracy compared to the ground part (from IT8 to IT9). On the basis of the achieved dimensional accuracy results, a coefficient of change in the degree of accuracy IT was created, which can be used to predict changes in the dimensional accuracy of ground surfaces after nitriding processes in degrees of accuracy IT3–IT10. In this study, a tool for predicting changes in degrees of accuracy of ground parts after nitriding processes is presented.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Metal and Thin Film Mechanics · Adhesion, Friction, and Surface Interactions · Surface Roughness and Optical Measurements

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Mechanical Engineering, Faculty of Military Technology, University of Defense, 662 10 Brno, Czech Republic

Department of Machining Technology, Institute of Manufacturing Technology, Faculty of Mechanical Engineering, Brno University of Technology, 616 69 Brno, Czech Republic

Department of Engineering Technologies and Materials, Faculty of Special Technology, Alexander Dubček University of Trenčín, 911 50 Trenčín, Slovakia

Funding

Project of Specific Research, Project for the Development of the Organization, Modern technologies for processing advanced materials used for interdisciplinary applications

References (72)

Show source-provided references
1. Improved wear resistance of AISI-1045 steel by hybrid treatment of plasma nitriding and post-oxidation10.1016/j.triboint.2022.107869 ↗
2. Tribological studies of dual-coating (intermediate hard with top epoxy-graphene-base oil composite layers) on tool steel in dry and lubricated conditions10.1016/j.triboint.2018.05.011 ↗
3. Enhanced surface properties of M2 steel by plasma nitriding pre-treatment and magnetron sputtered TiN coating10.1504/IJSURFSE.2020.112283 ↗
4. Comparison of tribological behaviours of AlCrN and TiAlN coatings—Deposited by physical vapour deposition10.1016/j.wear.2007.01.051 ↗
5. Prochazka, J., Pokorny, Z., and Dobrocky, D. (2020). Service behavior of nitride layers of steels for military applications. Coatings, 10.10.3390/coatings10100975 ↗
6. Influences of vacuum ion-nitriding on bending fatigue behaviors of 42CrMo4 steel: Experiment verification, numerical analysis and statistical approach10.1016/j.ijfatigue.2020.106104 ↗
7. Effect of nitriding and shot-peening on the fatigue behavior of 42CrMo4 steel: Experimental analysis and predictive approach10.1016/j.matdes.2011.09.055 ↗
8. Low temperature nitriding of AISI 300 and 200 series austenitic stainless steels10.1016/j.vacuum.2016.02.009 ↗
9. Nanomechanical properties of iron nitrides produced on 42CrMo4 steel by controlled gas nitriding and laser heat treatment10.1016/j.jallcom.2017.02.220 ↗
10. Influence of treatment time and temperature on surface property of active screen plasma-nitrided EN24 low alloy steel10.1007/s12666-021-02299-2 ↗
11. Effect of nitriding on mechanical and microstructural properties of Direct Metal Laser Sintered 17-4PH stainless steel10.1016/j.jmrt.2022.05.198 ↗
12. Effect of plasma nitriding in the corrosion behavior of an AISI 4140 steel using a seawater medium solution10.1016/j.matlet.2022.131991 ↗
13. Influence of current density on phase formation and tribological behavior of plasma nitrided AISI H13 steel10.1016/j.surfcoat.2015.12.025 ↗
14. Wear behavior of plasma nitride steels at ambient and elevated temperatures10.1016/S0043-1648(00)00426-9 ↗
15. Nitriding response of Cr alloyed steels10.1007/BF03258633 ↗
16. Influence of temperature and duration on the nitriding behavior of 40Cr low alloy steel in mixture of NH3 and N210.1016/j.surfcoat.2019.124953 ↗
17. Freudenberger, J., Göllner, J., Heilmaier, M., Mook, G., Saage, H., Srivastava, V., and Wendt, U. (2009). Material Science and Engineering. Springer Handbook of Mechanical Engineering, Springer.10.1007/978-3-540-30738-9_3 ↗
18. Verbindungsschichtbildung während des Gasnitrierens und des Gas- und Salzbadnitrocarburierens
19. Nucleation of iron nitrides during gaseous nitriding of iron: The effect of a preoxidation treatment
20. Mittemeijer, E.J., and Somers, M.A.J. (2015). Development of the compound layer during nitriding and nitrocarburizing of iron-carbon alloys. Thermochemical Surface Engineering of Steels, Woodhead Publishing.
21. Layer growth kinetics on gaseous nitriding of pure iron: Evaluation of diffusion coefficients for nitrogen in iron nitrides10.1007/BF02669794 ↗
22. Thermodynamics, kinetics and process control of nitriding10.1179/sur.1997.13.6.483 ↗
23. An opinion on the relationship between surface roughness and the prescribed dimensional tolerance of machine parts
24. Bumbalek, B., Odvody, V., and Ostadal, B. (1989). Surface Roughness, SNTL.
25. Cep, R., and Petru, J. (2013). Introduction to Machining Theory, Technical University of Ostrava.
26. Influence of the ratio gases and duration of the plasma nitriding on the changes texture of the surface34CrAl6 steel
27. Influence of chemical composition on layer properties of barrel steels
28. Plasma nitride compound layers in sintered parts: Microstructures and wear mechanisms10.1016/j.wear.2021.203810 ↗
29. Pokorny, Z. (2017). The Possibilities of Influencing the Basic Characteristics of the Layers during the Chemical-Thermal Treatment of Steels. [Habilitation Thesis, University of Defence].
30. Effect of nitrogen on surface morphology of layers
31. Mittemeijer, E., and Somers, M. (2015). Thermochemical Surface Engineering of Steels: Improving Materials Performance, Woodhead Publishing.10.3139/146.710019 ↗
32. Variation of the compound layer structure by controlled gas nitriding and nitrocarburizing10.1515/htm-2022-1011 ↗
33. The influence of active screen plasma nitriding parameters on corrosion behavior of a low-alloy steel10.1016/j.jallcom.2009.03.161 ↗
34. Modelling of layer development and nitrogen distribution on different microstructures during plasma nitriding10.1016/j.surfcoat.2022.128813 ↗
35. Pye, D. (2003). Practical Nitriding and Ferritic Nitrocarburizing, ASM International.10.31399/asm.tb.pnfn.9781627083508 ↗
36. A method to predict effective case depth in ion nitrided steels10.1016/j.surfcoat.2004.07.051 ↗
37. Surface properties of Fe4N compounds layer on AISI 4340 steel modified by pulsed plasma nitriding10.1016/j.jmst.2013.01.017 ↗
38. Characterization of the nitrided layers of XC38 carbon steel obtained by R.F. plasma nitriding10.1016/j.apsusc.2007.09.012 ↗
39. Enamel wear characterization based on a skewness and kurtosis surface roughness evaluation10.1016/j.biotri.2015.04.001 ↗
40. Modeling the effect of skewness and kurtosis on the static friction coefficient of rough surfaces10.1016/j.triboint.2003.11.010 ↗
41. Correlation between standard roughness parameters skewness and kurtosis and tribological behavior of contact surfaces10.1016/j.triboint.2011.11.008 ↗
42. Effect of directionality of unidirectional grinding marks on friction and transfer layer formation of Mg on steel using inclined scratch test10.1016/j.msea.2006.05.080 ↗
43. An experimental model for mixed friction during running-in10.1016/S0043-1648(02)00065-0 ↗
44. Effect of roughness parameter and grinding angle on coefficient of friction when sliding of Al-Mg alloy over EN8 steel10.1115/1.2345401 ↗
45. Chlebinova, L. (2016). Research on the Change in Dimension and Surface Roughness after Plasma Nitriding. [Ph.D. Thesis, Trenčianska Univerzita Alexandra Dubčeka].
46. Some effects of the plasma nitriding process on layer properties10.1016/0040-6090(92)90603-9 ↗
47. Wear properties of steel plasma nitrided at high temperatures10.1016/0921-5093(93)90269-K ↗
48. Tribological behaviour of plasma nitrided and plasma sulfonitrided cold work steels10.1179/174329404X7180 ↗
49. Laboratory assessment of wear on nitrided surfaces of dies for hot extrusion of aluminium10.1016/j.triboint.2005.09.032 ↗
50. Influence of the nitriding time in the wear behaviour of an AISI H13 steel during a crankshaft forging process10.1016/j.wear.2007.02.007 ↗
51. Sliding/rolling wear performance of plasma nitrided H11 hot working steel10.1016/j.triboint.2012.02.005 ↗
52. Microstructure and wear properties of AISI M2 tool steel on RF plasma nitriding at different N2-H2 gas compositions10.1016/j.surfcoat.2014.08.036 ↗
53. Microstructure and wear behaviour of pulsed plasma nitrided AISI H13 tool steel10.1080/00084433.2016.1241940 ↗
54. Effect of nitrided-layer microstructure control on wear behavior of AISI H13 hot work die steel10.1016/j.apsusc.2017.03.185 ↗
55. Effect of surface topography at different scales on the dispersion of the wetting data for sessile water droplets on nitrided austenitic stainless steels10.1016/j.surfcoat.2022.128510 ↗
56. Effect of N2 + H2 gas mixtures in plasma nitriding on tribological properties of duplex surface treated steels10.1016/j.matchar.2008.04.010 ↗
57. Mechanical and microstructural aspects of C20-steel blades subjected to gas nitriding10.1016/j.acme.2018.09.006 ↗
58. Tribological analysis of plasma nitrided SS310 steel material for different proces parameters
59. Totten, G.E. (1997). Nitriding Techniques and Methods. Steel Heat Treatment Handbook, Marcel Dekker, Inc.
60. Graf, M., and Holm, T. (2006). Furnace Atmospheres No. 3: Gas Nitriding and Nitrocarburizing, Linde AG.
61. Totten, G.E. (1997). Distortion of Heat-Treated Components. Steel Heat Treatment Handbook, Marcel Dekker, Inc.
62. Dosset, J., and Totten, G.E. (2013). Fundamentals of Nitriding and Nitrocarburizing. ASM Handbook 4A: Steel Heat Treatment Handbook, ASM International.
63. Dobrocky, D. (2015). Verification of Selected Mechanical Properties of Nitrided Layers of Structural Steels in a Wide Range of Temperatures. [Ph.D. Thesis, University of Defence].
64. Alloying element nitride development in ferritic Fe-based materials upon nitriding: A review10.1007/s11665-016-2048-x ↗
65. Surface roughness assessment on hole drilled trough the identification and clustering of relevant external and internal signal statistical features10.1016/j.cirpj.2021.11.007 ↗
66. The effect of surface roughness characteristics on the elastic-plastic contact performance10.1016/j.triboint.2014.05.016 ↗
67. Effect of Skewness and Roughness Level on the Mechanical Behavior of a Rough Contact
68. Influence of surface morphology and roughness on water wetting properties of low temperature nitrided auastenitic stainless steels10.1016/j.matchar.2014.07.006 ↗
69. Effect of surface roughness on the properties of the layer formed on AISI 304 stainless steel after plasma nitriding10.1016/j.surfcoat.2005.08.149 ↗
70. Influence of plasma-nitriding and surface roughness on the wear and corrosion resistance of thin films (PVD/PECVD)10.1016/j.surfcoat.2008.05.022 ↗
71. Evaluation of structural and mechanical properties of the nitrided layer on steel for weapons
72. Effects during plasma nitriding of shaped materials of different sizes10.1016/S0257-8972(02)00887-3 ↗