journal article·2021-01-23Open access

A Method for Accelerated Natural Weathering of Wood Subsurface and Its Multilevel Characterization

Anna Sandak, Jakub Sandak, Marion Noël, Athanasios Dimitriou

Coatings· Volume 11· Issue 2

Abstract

The function of altering weathering factors and degradation mechanisms are essential for understanding the weathering process of materials. The goal of this work was to develop a method for the acceleration of natural weathering and to investigate the molecular, microstructure and macrostructure degradation of wood caused by the process. Tests were performed in the whole month of July, which, according to previous research, is considered as the most severe for weathering of wood micro-sections. Sample appearance was evaluated by colour measurement. Scanning electron microscopy was used for evaluation of the structural integrity and changes in the microstructure of wood morphological components. Changes on the molecular level were assessed by means of FT-IR spectroscopy. Observation of the effects of weathering allowed a better understanding of the degradation process. Typical structural damage, such as cracks on bordered pits and cross-field pits, and, as a consequence, their erosion, revealed the sequence of the degradation process. It was confirmed that earlywood was more susceptible to damage than latewood. Even if the weathering test was conducted for a relatively short time (28 days) the ultra-thin wood samples changed noticeably. The progress of alteration was similar as usually noticed for wood surfaces, but occurred at shorter exposure times. The estimated acceleration factor was ×3, compare to the natural weathering kinetics of wood. The research methodology presented can be used for the determination of the weather dose-response models essential to estimate the future service life performance of timber elements.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Wood Treatment and Properties · Cultural Heritage Materials Analysis · Building materials and conservation

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Wood Modification, InnoRenew CoE, Livade 6, 6310 Izola, Slovenia

Faculty of Mathematics, Natural Sciences and Information Technologies, University of Primorska, Glagoljaška 8, 6000 Koper, Slovenia

Andrej Marušič Institute, University of Primorska, Titov trg 4, 6000 Koper, Slovenia

Institute Materials and Wood Technology, Bern University of Applied Sciences, Solothurnstrasse 102, Postfach 6096, CH-2500 Biel 6, Switzerland

The BioComposites Centre, Bangor University, Bangor, Gwynedd LL57 2UW, UK

Funding

Horizon 2020 Framework Programme · Ministerstvo školstva, vedy, výskumu a športu Slovenskej republiky

References (67)

Show source-provided references
1. Application of wood as an element of façade cladding in construction and reconstruction of architectural objects to improve their energy efficiency10.1016/j.enbuild.2015.03.047 ↗
2. Detection and distribution analysis of organosilicon compounds in wood by means of SEM-EDX and micro-CT10.1016/j.matchar.2005.09.007 ↗
3. Chemical and appearance changes of wood due to artificial weathering—Dose-response model10.1177/0967033518825364 ↗
4. Rowell, R.M. (2005). Weathering of wood. Handbook of Wood Chemistry and Wood Composites, CRC Press. [1st ed.].10.1201/9780203492437 ↗
5. (2021, January 03). Low-Temperature EMMA®/EMMAQUA®. Available online: https://www.atlas-mts.com/products/accelerated-weathering-test-services/natural-weathering/accelerated-weathering-test/emmaqua-weathering-test.
6. Application of microtensile testing to thin wood sections
7. Microtensile strength of spruce pine after exposure to acids and bases
8. Raczkowski, J. (1978, January 17–19). Natural atmospheric corrosion of microtome wood sections. Proceedings of the 10th Symp. on Wood Protection, Rogów, Poland. (In Polish).
9. Seasonal effects on the atmospheric corrosion of spruce micro-sections10.1007/BF02607398 ↗
10. (2018). BS EN 927-6 Paints and Varnishes. Coating Materials and Coating Systems for Exterior Wood, European Committee for Standardization.
11. Wood weathering in fluorescent ultraviolet and xenon arc chambers
12. A reliable artificial weathering test for wood coatings
13. Comparison of wood coating durability in natural weathering and artificial weathering using fluorescent UV-lamps and water10.1007/s00107-014-0791-y ↗
14. Comparing durability of wood material in natural and artificial weathering conditions
15. Color changes of wood and wood-based materials due to natural and artificial weathering10.1080/17480272.2012.696699 ↗
16. Modelling the outdoor performance of wood products—A review on existing approaches10.1016/j.conbuildmat.2014.05.087 ↗
17. External wood claddings—Performance criteria, driving rain and large-scale water penetration methods
18. Thiis, T.K., Burud, I., Kranitis, D., and Gobakken, L.R. (2016). Simulation of surface climate and mould growth on wooden facades. The International Research Group on Wood Protection IRG/WP 16-20585, IRG Secretariat.10.26868/25222708.2015.2939 ↗
19. Characterization and monitoring of surface weathering on exposed timber structures with multi-sensor approach10.1080/15583058.2015.1041190 ↗
20. Jones, D., and Brischke, C. (2017). Modelling of weathering. Performance of Bio-Based Building Materials, Woodhead Publishing. [1st ed.].
21. Wood morphology and properties from molecular perspectives10.1007/s13595-014-0403-3 ↗
22. Rowell, R.M. (2010). Structure and function of wood. Wood Handbook: Wood as an Engineering Material, Forest Products Laboratory.
23. Fengel, D., and Wegener, G. (1989). Wood—Chemistry, Ultrastructure, Reactions, Walter de Gruyter.
24. Structural quantification of wood fibre surfaces—Morphological effects of pulping and enzymatic treatment10.1016/j.micron.2010.03.002 ↗
25. Méndez-Vilas, A. (2012). Using SEM in monitoring changes in archaeological wood: A review. Current Microscopy Contributions to Advances in Science and Technology, Formatex Research Center.
26. Degradation assessment of waterlogged wood at Haimenkou site10.3221/IGF-ESIS.30.60 ↗
27. Wood degradation by Phellinus noxius: uItrastructure and cytochemistry10.1139/m95-035 ↗
28. Microscopic study of lime wood degraded by Chaetomium globosum
29. Visualising impregnated chitosan in Pinus radiata early wood cells using light and scanning electron microscopy10.1016/j.micron.2009.11.006 ↗
30. A novel approach for FE-SEM imaging of wood-matrix polymer interface in a biocomposite10.1016/j.micron.2013.08.011 ↗
31. Structural and fractographic SEM analysis of exterior coated wood10.1007/BF02699699 ↗
32. Weathering characteristics of wood treated with water glass, siloxane or DMDHEU10.1007/s00107-011-0520-8 ↗
33. Kocaefe, D., Huang, X., and Kocaefe, Y. (2013, January 25–27). Comparison of weathering behaviours of heat-treated jack pine during different artificial weathering conditions. Proceedings of the 4th International Conference on Fluid Mechanics and Heat & Mass Transfer (FLUIDSHEAT’13), Dubrovnik, Croatia.
34. Ganne-Chedeville, C., Volkmer, T., Letsch, B., and Lehmann, M. (2012, January 15–19). Measures for the maintenance of untreated wood facades. Proceedings of the WCTE, Auckland, New Zealand.
35. How spectroscopy and microspectroscopy of degraded wood contribute to understand fungal wood decay10.1007/s00253-012-4369-5 ↗
36. Assessment of wood structural members degradation by means of infrared spectroscopy: An overview10.1002/stc.1777 ↗
37. Structural changes in biodegraded lime wood10.1016/j.carbpol.2009.08.015 ↗
38. Structural modifications of Tilia cordata wood during heat treatment investigated by FT-IR and 2D IR correlation spectroscopy10.1016/j.molstruc.2012.08.035 ↗
39. Distinction of three wood species by Fourier transform infrared spectroscopy and two-dimensional correlation IR spectroscopy10.1016/j.molstruc.2007.11.061 ↗
40. Weathering kinetics of thin wood veneers assessed with near infrared spectroscopy10.1255/jnirs.1230 ↗
41. Application of extended inverse scatter correction to mid-infrared reflectance spectra of soil10.1002/cem.929 ↗
42. Classification of lignins from different botanical origins by FT-IR spectroscopy10.1515/hfsg.1991.45.s1.21 ↗
43. Effects of short-time vibratory ball milling on the shape of FT-IR spectra of wood and cellulose10.1016/j.vibspec.2004.02.003 ↗
44. Degradation of lime wood painting supports II. Spectral characterisation
45. Using NIR and ATR-FTIR spectroscopy to rapidly detect compression wood in Pinus radiata10.1139/cjfr-2013-0329 ↗
46. In situ micro-FTIR observation of molecular association of adsorbed water with heat-treated wood10.1007/s00226-018-1020-3 ↗
47. Evaluation of degradation in chemical compounds of wood in historical buildings using FT-IR and FT-Raman vibrational spectroscopy
48. Noda, I., and Ozaki, Y. (2005). Two-Dimensional Correlation Spectroscopy, John Willey & Sons Ltd.
49. Two-dimensional infrared spectroscopy10.1021/ja00203a008 ↗
50. Effect of angle of exposure on the weathering of wood surfaces10.1016/0141-3910(89)90135-3 ↗
51. Wood degradation under UV irradiation: A lignin characterization10.1016/j.jphotobiol.2016.02.030 ↗
52. Artificial weathering of tropical woods. Part1: Changes in wettability10.1515/HF.2004.084 ↗
53. (2000). EN 927-3 Paints and Varnishes—Coating Materials and Coating Systems for Exterior Wood—Part 3: Natural Weathering Test, European Committee for Standardization.
54. Yellowing and IR-changes of spruce wood as result of UV-irradiation10.1016/S1011-1344(02)00412-8 ↗
55. Artificial ageing of wood monitored by DRIFT spectroscopy and CIE L*a*b* colour measurements10.1515/hfsg.1995.49.5.397 ↗
56. Turkulin, H. (2004). SEM Methods in Surface Research on Wood, CTBA. COST E 18 Final Seminar.
57. Weathering of radial and tangential wood surfaces of pine and spruce10.1515/HF.1999.059 ↗
58. Weathering characteristics of modified rubberwood (Hevea brasiliensis)10.1002/app.10667 ↗
59. Scanning electron microscope and infrared studies of weathering in southern pine10.1016/0022-2860(93)87010-7 ↗
60. Comparative study of photodegradation of six wood species after short-time UV exposure10.1007/s00226-015-0771-3 ↗
61. Laane, J. (2017). Advances in two-dimensional correlation spectroscopy (2DCOS). Frontiers and Advances in Molecular Spectroscopy, Elsevier Science Publishing Co Inc.. [1st ed.].
62. Grossman, D., and Ketola, W. (1994). Errors caused by using Joules to time laboratory and outdoor exposure tests. Accelerated and Outdoor Durability Testing of Organic Materials, ASTM International.10.1520/STP1202-EB ↗
63. Burud, I., Sandak, A., Sandak, J., Flö, A., Thiis, T., Gobakken, R.L., Smeland, K.A., and Kvaal, K. (2015, January 18–23). Weather degradation of thin wood samples assessed with NIR hypersepctral imaging in transmission mode. Proceedings of the 17th International Conference on Near Infrared Spectroscopy, Foz do Iguassu, Brazil.10.17648/nir-2015-34156 ↗
64. Weathering characteristics of Australian grown radiata pine
65. Wang, Y., Zhu, W., Zhang, X., Cai, G., and Wan, B. (2020). Influence of thickness on water absorption and tensile strength of BFRP Laminates in water or alkaline solution and a thickness-dependent accelerated ageing method for BFRP laminates. Appl. Sci., 10.10.3390/app10103618 ↗
66. Accelerated climate ageing of building materials, components and structures in the laboratory10.1007/s10853-012-6349-7 ↗
67. Jankowska, A., Rybak, K., Nowacka, M., and Boruszewski, P. (2020). Insight of weathering processes based on monitoring surface characteristic of tropical wood species. Coatings, 10.10.3390/coatings10090877 ↗