The Microstructure and Selected Mechanical Properties of Al2O3 + 13 wt % TiO2 Plasma Sprayed Coatings
Source abstract
Abstract
The Al2O3 + TiO2 coatings are of the interest of surface technology and tribology due to their good wear resistance and enhanced toughness comparing to pure Al2O3 coatings. However, the detailed effect of the used feedstock powder, is often neglected. Here, this work focuses on the deposition of Al2O3 + 13 wt % TiO2 coatings by atmospheric plasma spraying (APS) method as well as on their microstructure, phase composition and selected mechanical properties, in the reference to the route of the powder feedstock preparation. The commercial powder Metco 6221 in agglomerated and sintered form was used as a feedstock material during spraying, due to the fact that, so far, sintered or cladded powders are the most studied ones. The 2k + 1 spray experiment allowed to evaluate the influence of two variables, namely spray distance and torch linear velocity, on the coating microstructure. Afterwards, the coating adhesion was measured by the means of pull-off test. The correlations between Vickers microhardness, fracture toughness (Kc) as well as the coating morphology and phase composition were investigated. Finally, the dry sliding wear resistance was studied by using Ball-on-Disc method.
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Research context
OpenAlex topics: High-Temperature Coating Behaviors · Metal and Thin Film Mechanics · Advanced ceramic materials synthesis
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Faculty of Mechanical Engineering, Wrocław University of Science and Technology, Łukasiewicza 5, 50-371 Wrocław, Poland
References (41)
Show source-provided references
1. Impact of Plasma Spray Variables Parameters on Mechanical and Wear Behaviour of Plasma Sprayed Al2O3 3% wt TiO2 Coating in Abrasion and Erosion Application10.1016/j.proeng.2012.07.369 ↗
2. Influence of the feedstock characteristics on the microstructure and properties of Al2O3–TiO2 plasma-sprayed coatings10.1016/j.surfcoat.2012.09.042 ↗
3. Tribological properties of thermal spray coatings
4. Tribological behavior of plasma sprayed Cr2O3–3%TiO2 coatings—ScienceDirect10.1016/j.wear.2011.08.004 ↗
5. A design of experiment study of plasma-sprayed alumina-titania coatings10.1007/BF02650473 ↗
6. Microstructures and Functional Properties of Suspension-Sprayed Al2O3 and TiO2 Coatings: An Overview10.1007/s11666-009-9417-z ↗
7. Szala, M., Walczak, M., Pasierbiewicz, K., and Kamiński, M. (2019). Cavitation Erosion and Sliding Wear Mechanisms of AlTiN and TiAlN Films Deposited on Stainless Steel Substrate. Coatings, 9.10.20944/preprints201904.0228.v1 ↗
8. Abrasion, Erosion and Cavitation Erosion Wear Properties of Thermally Sprayed Alumina Based Coatings10.3390/coatings4010018 ↗
9. Atmospheric plasma sprayed (APS) coatings of Al2O3–TiO2 system for photocatalytic application10.1039/b817199h ↗
10. Microstructural transformations of TiO2, Al2O3+13TiO2 and Al2O3+40TiO2 at plasma spraying and laser engraving10.1016/j.surfcoat.2004.01.010 ↗
11. Microstructure and tribological properties of nanostructured and conventional plasma sprayed alumina–titania coatings10.1016/j.surfcoat.2014.09.014 ↗
12. Microstructure, Corrosion, and Fatigue Properties of Alumina-Titania Nanostructured Coatings
13. Comparative wear study of plasma sprayed TiO2 and Al2O3–TiO2 on mild steels—ScienceDirect10.1016/j.triboint.2015.05.001 ↗
14. Emergence and impact of Al2TiO5 in Al2O3-TiO2 APS coatings
15. Microstructure development of Al2O3–13 wt % TiO2 plasma sprayed coatings derived from nanocrystalline powders10.1016/S1359-6454(01)00414-1 ↗
16. Study of the microstructure of plasma sprayed coatings obtained from Al2O3–13TiO2 nanostructured and conventional powders10.1016/j.matchar.2014.08.016 ↗
17. Fabrication and evaluation of plasma sprayed nanostructured alumina–titania coatings with superior properties10.1016/S0921-5093(00)01382-4 ↗
18. Indentation fracture behavior of plasma-sprayed nanostructured Al2O3–13 wt.%TiO2 coatings10.1016/S0921-5093(02)00523-3 ↗
19. Pawłowski, L. (2008). The Science and Engineering of Thermal Spray Coatings, Wiley. [2nd ed.].10.1002/9780470754085 ↗
20. Fauchais, P.L., Heberlein, J.V.R., and Boulos, M. (2014). Thermal Spray Fundamentals: From Powder to Part, Springer.10.1007/978-0-387-68991-3 ↗
21. Microstructure and mechanical properties of plasma sprayed Al2O3—13%TiO2 Ceramic Coating10.1051/matecconf/20178702027 ↗
22. Suspension and solution thermal spray coatings10.1016/j.surfcoat.2009.03.005 ↗
23. (2014). ASTM E2109-01 01 Standard Test Methods for Determining Area Percentage Porosity in Thermal Sprayed Coatings, ASTM.
24. (2004). EN ISO 4516: 2004 Metallic and other Inorganic Coatings—Vickers and Knoop Microhardness Tests, Swiss Association for Standardization.
25. Occurrence of crack formation during Vickers indentation as a measure of the toughness of hard materials
26. A fracture mechanics analysis of indentation-induced Palmqvist crack in ceramics10.1007/BF00725625 ↗
27. A Critical Evaluation of Indentation Techniques for Measuring Fracture Toughness: II, Strength Method10.1111/j.1151-2916.1981.tb10321.x ↗
28. Twadość Vickersa i odporność na pękanie wybranych kompozytów ceramicznych
29. Comparison of mechanical properties of the plasma sprayed coatings by powder and suspension
30. (2016). ASTM G99-17 Standard Test Method for Wear Testing with a Pin-on-Disk Apparatus, ASTM.
31. Mechanical and tribological performance of Al2O3-TiO2 coatings elaborated by flame and plasma spraying - ScienceDirect10.1016/j.surfcoat.2010.07.061 ↗
32. An evaluation of plasma-sprayed coatings based on Al2O3 and Al2O3–13wt.% TiO2 with bond coat on pure titanium substrate10.1016/j.ceramint.2008.11.017 ↗
33. Comparative Study on Nano-Structural and Traditional Al2O3-13TiO2 Air Plasma Sprayed Coatings and their Thermal Shock Performance10.4028/www.scientific.net/KEM.739.103 ↗
34. The anatase-rutile transition. Part 1—Kinetics of the transformation of pure anatase10.1039/TF9585401069 ↗
35. Pressure-temperature studies of anatase, brookite, rutile and TiO2-II
36. The dependency of microstructure and properties of nanostructured coatings on plasma spray conditions10.1016/S0257-8972(00)00673-3 ↗
37. Thermisch gespritzte Schichten im System Al2O3–Cr2O3–TiO2—Ein Update10.1002/mawe.201400260 ↗
38. Freudenberg, F. (1988). Etude de la réaction à l’état solide Al2O3 + TiO2 → Al2TiO5: Observation des structures: ThéseVÉ cole polytechnique fe´de´rale de Lausanne EPFL. EPFL Lausanne, 709.
39. Berger, L.-M. (2015). Tribology of thermally sprayed coatings in the Al2O3-Cr2O3-TiO2 system. Thermal Sprayed Coatings and Their Tribological Performances, IGI Global. Engineering Science Reference.10.4018/978-1-4666-7489-9.ch008 ↗
40. Tribological properties of Al2O3+ TiO2 coatings manufactured by plasma spraying
41. Fabrication and properties of plasma-sprayed Al2O3/TiO2 composite coatings: A role of nano-sized TiO2 addition10.1016/j.surfcoat.2009.10.052 ↗