Magnesium Doped Hydroxyapatite-Based Coatings Obtained by Pulsed Galvanostatic Electrochemical Deposition with Adjustable Electrochemical Behavior
Source abstract
Abstract
The aim of this study was to adapt the electrochemical behavior in synthetic body fluid (SBF) of hydroxyapatite-based coatings obtained by pulsed galvanostatic electrochemical deposition through addition of Mg in different concentrations. The coatings were obtained by electrochemical deposition in a typical three electrodes electrochemical cell in galvanic pulsed mode. The electrolyte was obtained by subsequently dissolving Ca(NO3)2·4H2O, NH4H2PO4, and Mg(NO3)2·6H2O in ultra-pure water and the pH value was set to 5. The morphology consists of elongated and thin ribbon-like crystals for hydroxyapatite (HAp), which after the addition of Mg became a little wider. The elemental and phase composition evidenced that HAp was successfully doped with Mg through pulsed galvanostatic electrochemical deposition. The characteristics and properties of hydroxyapatite obtained electrochemically can be controlled by adding Mg in different concentrations, thus being able to obtain materials with different properties and characteristics. In addition, the addition of Mg can lead to the control of hydroxyapatite bioactive ceramics in terms of dissolution rate.
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Research context
OpenAlex topics: Bone Tissue Engineering Materials · Titanium Alloys Microstructure and Properties · Advanced materials and composites
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Faculty of Materials Science and Engineering, University Politehnica of Bucharest, RO060042 Bucharest, Romania
Faculty of Dental Medicine, University of Medicine and Pharmacy “Carol Davila”, RO020021 Bucharest, Romania
Department for Advanced Surface Processing and Analysis by Vacuum Technologies, National Institute of Research and Development for Optoelectronics-INOE 2000, RO77125 Magurele, Romania
National Research Tomsk Polytechnic University, 634050 Tomsk, Russia
Funding
Operational Program Human Capital of the Ministry of European Funds through the Financial Agreement · Romanian Ministry of Research and Innovation, CCCDI – UEFISCDI, projects number COFUND-ERANET-RUS-PLUS-CoatDegraBac · Core Program of 2019 · PROINSTITUTIO Project–contract
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