Functionalization of mesoporous silica surface with carboxylic groups by Meldrum’s acid and its application for sorption of proteins
Source abstract
Abstract
A new method of silica surface functionalization with carboxyl groups is proposed based on the reaction between 2,2-dimethyl-1,3-dioxane-4,6-dione (Meldrum’s acid, MA) and the surface silanol groups. For the first time such a post-synthesis modification was successfully applied to silica materials. Although silica surface is successfully carboxylated (as evidenced by FTIR and XPS), the porosity, ordering and morphology remain practically unchanged after the proposed post-synthesis treatment (as confirmed by nitrogen sorption, XRD and electron microscopy). Adsorption study of model biomolecules (lysozyme and bovine serum albumin) shows that different surface chemistries (–OH vs. –COOH) lead to different affinities between the silica surface and sorbates.
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Research context
OpenAlex topics: Mesoporous Materials and Catalysis · Analytical Chemistry and Chromatography · Diatoms and Algae Research
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (67)
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