journal article·2003-08-01

Large-Scale Preparation of Solubilized Carbon Nanotubes

Yujun Qin, Luqi Liu, Jiahua Shi, Wei Wu, Jun Zhang, Zhi-Xin Guo, Yongfang Li, Daoben Zhu

Chemistry of Materials· Volume 15· Issue 17
Publisher page

Abstract

We report here a method that can be used to easily prepare bulk quantities of solubilized carbon nanotubes. The method is derived from Haddon's method in which we have modified the separation process by using two Soxhlet extractors in the procedure. Both primary and secondary amines could be used as starting materials to solubilize carbon nanotubes in our process, and the solubilized multiwalled carbon nanotubes (MWNTs) were fully characterized. Owing to the large quantity of solubilized MWNTs obtained, several basic properties such as the solubility and the percentage content of tubes in the solubilized samples have been determined and analyzed. Typical solubilized MWNT/polymer composites were also fabricated and their electronic and thermal properties were investigated.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Carbon Nanotubes in Composites · Fullerene Chemistry and Applications · Graphene research and applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, China, and Graduate School of Chinese Academy of Sciences, Beijing 100080, China

References (31)

Show source-provided references
1. Special Issue on Carbon Nanotubes.Acc. Chem. Res.2002,35(12).10.1021/ar010166k ↗
2. Ajayan M. · Chem. Rev. · 1999 · 99 · 178710.1021/cr970102g ↗
3. Yakobson B. I. · Am. Sci. · 1997 · 85 · 324
4. Gong X. · Chem. Mater. · 2000 · 12 · 104910.1021/cm9906396 ↗
5. Andrews R. · Appl. Phys. Lett. · 1999 · 75 · 132910.1063/1.124683 ↗
6. Rao A. M. · Appl. Phys. Lett. · 2000 · 76 · 381310.1063/1.126790 ↗
7. Gao B. · Adv. Mater. · 2001 · 13 · 177010.1002/1521-4095(200112)13:23<1770::AID-ADMA1770>3.0.CO;2-G ↗
8. Sun X. · Appl. Phys. Lett. · 1998 · 73 · 363210.1063/1.122845 ↗
9. Chen P. · Phys. Rev. Lett. · 1999 · 82 · 254810.1103/PhysRevLett.82.2548 ↗
10. Tang B. Z. · Macromolecules · 1999 · 32 · 256910.1021/ma981825k ↗
11. Ouyang, M.; Huang, J.L.; Lieber, C. M.Acc. Chem. Res.2002,35, 1018, and references therein.10.1021/ar0101685 ↗
12. Star A. · Angew. Chem., Int. Ed. · 2001 · 40 · 172110.1002/1521-3773(20010504)40:9<1721::AID-ANIE17210>3.0.CO;2-F ↗
13. Ago H. · Adv. Mater. · 1999 · 11 · 128110.1002/(SICI)1521-4095(199910)11:15<1281::AID-ADMA1281>3.0.CO;2-6 ↗
14. For · J. Mater. Chem. · 2002 · 12 · 195210.1039/b201013p ↗
15. Chen J. · Science · 1998 · 282 · 9510.1126/science.282.5386.95 ↗
16. Georgakilas V. · J. Am. Chem. Soc. · 2001 · 124 · 76010.1021/ja016954m ↗
17. Liu L. Q. · Chem. Phys. Lett. · 2002 · 359 · 19110.1016/S0009-2614(02)00710-8 ↗
18. Hamon M. A. · Adv. Mater. · 1999 · 11 · 83410.1002/(SICI)1521-4095(199907)11:10<834::AID-ADMA834>3.0.CO;2-R ↗
19. Chen J. · J. Phys. Chem. B · 2001 · 105 · 252510.1021/jp002596i ↗
20. Pompeo F. · Nano Lett. · 2002 · 2 · 36910.1021/nl015680y ↗
21. Kahn M. G. C. · Nano Lett. · 2002 · 2 · 121510.1021/nl025755d ↗
22. Basiuk E. V. · J. Phys. Chem. B · 2002 · 106 · 158810.1021/jp0120110 ↗
23. Luque de Castro M. D. · Anal. Chim. Acta · 1998 · 369 · 110.1016/S0003-2670(98)00233-5 ↗
24. Tan P. · J. Raman Spectrosc. · 1997 · 28 · 36910.1002/(SICI)1097-4555(199705)28:5<369::AID-JRS107>3.0.CO;2-X ↗
25. Li W. · Appl. Phys. Lett. · 1997 · 70 · 268410.1063/1.118993 ↗
26. Hiura H. · Chem. Phys. Lett. · 1993 · 202 · 50910.1016/0009-2614(93)90040-8 ↗
27. Ando Y. · Carbon · 2001 · 39 · 56910.1016/S0008-6223(00)00162-7 ↗
28. Bom D. · Nano Lett. · 2002 · 2 · 61510.1021/nl020297u ↗
29. Sivaraman N. · J. Org. Chem. · 1992 · 57 · 607710.1021/jo00048a056 ↗
30. Bahr J. L. · Chem. Commun. · 2001 · 19310.1039/b008042j ↗
31. Ruoff R. S. · J. Phys. Chem. · 1993 · 97 · 337910.1021/j100115a049 ↗