Pressure-Controlled Fabrication of Stibnite Nanorods by the Solvothermal Decomposition of a Simple Single-Source Precursor
Source abstract
Abstract
A simple single-source precursor to stibnite (Sb 2 S 3 ) synthesized from SbCl 3 and thiourea in methanol was characterized. The thermal decomposition of the precursor in polar solvents resulted in the formation of one-dimensional Sb 2 S 3 nanocrystallites with the growth direction along the c axis. It is found that the as-prepared Sb 2 S 3 nanorods are formed through the spontaneous connection of adjacent particles. The pressure in the solvothermal process plays an important role in the formation of the nanorods.
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Research context
OpenAlex topics: Chalcogenide Semiconductor Thin Films · Quantum Dots Synthesis And Properties · Crystal Structures and Properties
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Affiliations
Department of Chemistry, and Structure Research Laboratory, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China
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