journal article·2007-09-01

Electrosynthesis of Thin Films of Ni, Al Hydrotalcite Like Compounds

Erika Scavetta, Adriana Mignani, Daria Prandstraller, Domenica Tonelli

Chemistry of Materials· Volume 19· Issue 18
Publisher page

Abstract

Thin films of pure-nickel-based hydrotalcite-like compounds have been deposited on a Pt electrode by electrosynthesis. The best films have been obtained by cathodic reduction of a 0.03 M solution of Ni and Al nitrates in different molar ratios. The films, obtained in different experimental conditions, have been characterized by different techniques, such as SEM, AFM, and XRD. Particular attention has been devoted to understanding the mechanism of their growth. The electrochemical properties of the films obtained for different deposition times and Ni/Al ratios have been studied in basic solution (NaOH) by cyclic voltammetry and AC impedance spectroscopy.
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Research context

OpenAlex topics: Layered Double Hydroxides Synthesis and Applications · Supercapacitor Materials and Fabrication · Thermal Expansion and Ionic Conductivity

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Physical and Inorganic Chemistry, University of Bologna, Viale Risorgimento 4, 40136 Bologna, INSTM, UdR Bologna, Italy, and Microchemistry and Microscopy Art Diagnostic Laboratory (M2ADL),University of Bologna, Ravenna Campus, Via Tombesi dall' Ova 55, 48100 Ravenna, Italy

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