journal article·2021-03

Synthesis of activated carbon in the presence of hydrochar from chickpea stalk and its characterization

Dicle University, Diyarbakir Vocational School Of Technical Sciences, Chemical and Chemical Processing Technologies, Diyarbakır,, Turkey, 21280, N. Genli, Ö. Şahin, Siirt University, Engineering Faculty, Department of Chemical Engineering, Siirt, Turkey, 56100, O. Baytar, Siirt University, Engineering Faculty, Department of Chemical Engineering, Siirt, Turkey, 56100, S. S., Siirt University, Engineering Faculty, Department of Electrical and Electronics, Siirt, Turkey, 56100

Journal of Ovonic Research· Volume 17· Issue 2
Publisher page

Abstract

In this study, hydrochar was obtained from chickpea stalk by hydrothermal method. Then, activated carbon was synthesized by chemical activation method using ZnCl2 activator in the presence of this hydrochar. The effects of parameters such as impragnation rate (hydrochar/ZnCl2), impragnation rate, activation temperature and activation time on activated carbon synthesis were investigated. The iodine number of the obtained activated carbon was determined and its characterization was performed by SEM, BET, FTIR measurements. It was determined that the highest iodine number of synthesized activated carbon was 734 mg/g under conditions of impragnation time (24 hour), impragnation rate (1/2), activation temperature (400 oC), and activation time (45 minutes). The BET surface area of the activated carbon with the highest iodine number was determined as 572 m2 /g. The methylene blue number of synthesized activated carbon and hydrochar were found as 105 mg/g and 45 mg/g, respectively.
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Research context

OpenAlex topics: Boron and Carbon Nanomaterials Research · Graphene and Nanomaterials Applications · Polymer Nanocomposite Synthesis and Irradiation

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